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GCMS analysis results for sample AE10245, May 28, 2002

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Laboratory report documenting GCMS analysis of sample AE10245 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024863–000024870

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document Llbrary searen compound Report

Data File : C:\MSDCHEM\1\DATA\020509\10245.D Vial: 23 Acq On : 10 May 2002 8:22 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.37 ug/1 40590 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 001719-06-8 64 188 C14D10 2 Phenanthrene-diO 001517-22-2 50 188 C14D10 3 3,4-Oxazolidinecarboxylic acid, ... 245 C11H19NO5 116842-10-5 25 4 7-Norcarancarbonic acid, methyl e. . . 154 C9H14O2 1000222-16-2 10 Abundance Scan 4916 (31.964 min): 10245.D (-4908) (-) m/z 188.15 100.00% 188

5000 80 / 94 158 40 66 31.60 31.80 32.00 32.20 =111,41 ,108.132., , ..... I > > i i ' 1 ।-| 1 * ■ > । m/ z 80.30 23.41% m/z->20 40 60 80 100 120 140 160 180 200 220 Abundance #79826: Anthracene-d10- 188

5000 31.60 31.80 32.00 32.20 m/Z 184.20 18.21% 80 94 160

m/z->20 17 28 40 52 40 T I60 66 —1104 80 100 118.132,146.179, 120 140 160 al— 180 200 220 1 ■ i ' ■ 1 1 i

Abundance #79827: Phenanthrene-d10 188

31.60 31.80 32.00 32.20 5000 m/z 93.90 17.70%

80 94 160 2840, 52,6614 1 108 120 132 146 I • 179,4 .... ■ ' i ■ ' ■ ' i nz-> 20 40 60 801 100 120 140 160 180 200 220 Abundance #79684:3,4-Oxazolidinecarboxylic acid, 2-(1,1-dimethyleth... 188 31.60 31.80 32.00 32.20 m/z 158.05 15.40% 5000

42 88 56 144 29 J..T 100 116128 I 160170 THT—tr 1 1 1" | 214 230 ——— I’I’III — m/z—> 20 40 60 80 100 120 140 160 180 200 220 31.60 31.80 32.00 32.20

10245.D SCAN020507.M Tue May 14 14:26:33 2002 Page 5

NYC-WTC_000024869

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NYC-WTC_000024869Source: NYC Law Department, mirrored locally

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