GCMS quantitation results for sample AE10241, May 2002

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Laboratory report of GCMS analysis for sample AE10241 conducted on May 28, 2002.

NYC-WTC_000024770–000024779

Folder label: “GCMS X 5/14/02 A 5/17/02”

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NYC 9/11 Public Portal Document Llbrary searen compound Report

Data File : C:\MSDCHEM\1\DATA\020516\10241.D Vial: 17 Acq On : 17 May 2002 1:10 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.31 ug/1 21718 Phenanthrene-dl0 31.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 64 2 Phenanthrene-d10 188 C14D10 001517-22-2 42 3 Antipyrine 188 C11H12N2O 000060-80-0 32 4 Antipyrine 188 C11H12N2O 000060-80-0 9 Abundance Scan 4914 (31.952 min): 10241.D (-4907) (-) m/z 188.20 100.00% 188

5000 80 94 66 118 158 54 —l 31.60 31.80 32.00 32.20 -44 H aa lid ■ 1111111111 ((111 < । > > 11111 < ■ 1111 ar m/ z 189.10 31.03% miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 158

5000 31.60 31.80 32.00 32.20 m/z 80.00 30.35% 80 94 160 . | 17 30 42 52 I 66 | 108118 132 146 I, 170179 ‘i । n-rr| 11 M-p i 11111 n 111 < i TH 11" r 111.. | ■ mi . n-rT. ■, TTNTNThr Wr n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-dio 188 ............... ........................................

31.60 31.80 32.00 32.20 5000 m/z 94.20 26.83%

80 94 160 30 42 52 66 , 108 118 132 146 11, 1701791,1 'i | .-n-, । , , ■ , p-r-. , | I, ,-ti-H i , । , Hi | i, ll r. ■ 11 11 TmmTTT mz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79725: Antipyrine 4. — ,, . 11 1(18 31.60 31.80 32.00 32.20 96 m/z 158.10 18.83% 5000 77 56 /....................•.................. 105 27 39 I I 67 . Il 115 130 145 159 173 i mmH -HH+ '' i' I’l i11111'1 ■ ■ 'T1' "i11111 ''l ।1111" ।11111IL rTp-rrr mfz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10241.D SCAN020507.M Fri May 17 10:39:54 2002 Page 5

NYC-WTC_000024778

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