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GCMS blank results for sample AE11157, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing blank test results for GCMS analysis of sample AE11157 conducted between May 13 and May 16, 2002.

NYC-WTC_000024629–000024639

Folder label: “GCMS X 5/13/02 A 5/15/02

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NYC 9/11 Public Portal Document Library searcn compound Report

Data File : C:\MSDCHEM\1\DATA\020515\0513LB1.D Vial: 3 Acq On : 15 May 2002 1:48 pm Operator: Nefliu Sample : 05/13 lab blk Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.36 ug/1 34048 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 53 2 1,4-Naphthalenedione, 2-hydroxy-... 188 C11H803 000483-55-6 43 3 Benzaldehyde, 2,6-difluoro-4-hyd... 188 C8H6F2O3 1000116-28-9 25 4 1,4- phthalenedione, 5-hydroxy- . . . 188 C11H803 000481-42-5 9 Abundance Scan 4916 (31.964 min): 0513LB1 .D (-4908) (-). m/z 188.15 100.00% 188

5000 80 94 158 44 55 64 104 31.60 31.80 32.00 32.20 ['l ■'■'I"-" I " .l|. I'M 'I ■I"l" ill'll __ ______________ siloanyonnsyli H m/ z 80.00 25.65% ’ i1" ■ i " " i ‘ "1111 "i " " i vJz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d1 0- 188

5000 31.60 31.80 32.00 32.20 m/z 189.20 21.49% 80 94 160 | 17 30 42 52 7 J 108118 132 146 II 170179 L| | ii I । | । 1 i « j i i । I | I i i I | I I I । | I I 1 । j i i 1 1 J I I । I | I I i | [ I । I I | 11 I I | I I I | | I ! t ! | J I I I J I 1 PI j'l ! I I | I | I | |'| PI TTIT mfz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125707:1,4-Naphthalenedione, 2-hydroxy-3-methyl- 188

31.60 31.80 32.00 32.20 5000 m/z94.10 21.25%

50 77 105 131 160

n/z-> ■ ।" " ।" " । ■"11 ■ ■" 1'"'' —... L........ 1 15... H........ I....... 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TTT ' I ,/........................................ Abundance #79823: Benzaldehyde, 2,6-difluoro-4-hydroxy-3-methoxy- 188 31.60 31.80 32.00 32.20 m/z 158.10 16.84% 5000 173 43 57 69 78 88 97 117 , 145 mZz-> --4llFhH2HP,MH —— TT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

0513LB1.D SCAN020507.M Thu May 16 14:43:14 2002 Page 7

NYC-WTC_000024638

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NYC-WTC_000024638Source: NYC Law Department, mirrored locally

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GCMS sample preparation log, May 2002 · Box DEP Box 18

NYC-WTC_000024427

Record of sample preparation parameters including drip rates and volumes for GCMS analysis conducted in mid-May 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.990

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