GCMS results for sample AE11427, May 29, 2002

NYC 9/11 Public Portal Document LibrarY searcn compound Report

Data File : C:\MSDCHEM\l\DATA\020521\11427.D Vial: 13 Acq On : 21 May 2002 8:13 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.29 ug/1 29513 Phenanthrene-dl0 31.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 87 2 P tacyclo[7.3.1.1. (4,12).0(2,7)... 188 C14H20 1000215-61-8 58 3 A tipyrine 188 C11H12N2O 000060-80-0 53 4 44Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 53 Abundal Scan 4916 (31.963 min): 11427.D (-4907) (-) m/z 188.20 100.00% its

5000

44 54 67 80 92 160 170 3160 31,80 32.00 32.20 0 --------------- m/z 187.25 14.72% n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 . — ! I r i । ! i i . । i

5000 31.60 31.80 32.00 32.20 m/z 188.90 13.80% or 80 94 iso 17 30 42 52 ° 108118 132 146 1 170179 0 TITITTCktthu mfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1.(4,12).0(2,7).0(6,11)]tetradeca... US 1II ■ • • • i > • ■ ■ । . 31.60 31.80 32.00 32.20 5000 79 91 m/z 79.80 10.21% 55 67 105 117 131 145 159 niz-> 0- ■ i' • ■ ■ i ‘। ■ i ■ ■" ।111 ■ ।' 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 JU 173" i “ ■ I ■ i

Abundance #125690: Antipyrine ■ ■ i US 31.60 31.80 32.00 32.20 m/ z 92.30 9.97% 96 5000 77 56 105 431!'. ■ | ,i'l 1ri 67 159 173 | m/z—> 0 ,........ ... . i. ■ ■ 111! - 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 U . I r . . q-T-i TTT" 31,60 31.80 32.00 32.20 4 11II

11427.D SCAN020521.M Fri May 24 09:30:36 2002 Page 6

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