GCMS analysis results for sample AE11285, May 2002

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Data File : C:\MSDCHEM\1\DATA\020516\11285.D Vial: 13 Acq On : 16 May 2002 9:13 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.28 ug/1 21552 Phenanthrene-dl0 31.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 001719-06-8 45 188 C14D10 2 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) . . . 188 C14H20 1000215-61-8 43 3 Benzene, 1-(1-cyclohexen-l-yl)-4... 188 C13H160 020758-60-5 9 4 3-^ ino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 9 Abundance Scan 4915 (31.958 min): 11285.D (-4906) (-) m/z 188.20 100.00% 188

5000 94 44 54 66 78 146 156 3160 31.80 32.00 32.20 TTTTTTTTTTTTTTT 1' I' 11 i’T H m/z 94.00 22.97% m/z-? 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 ■ I r ■ | ■ I . . n । । > < > । । ■ , > । > 31.60 31.80 32.00 32.20 m/z 189.10 20.97% 66 80 94 160 17 30 42 52 I' " ''I'' '~l~ ‘" l" " I " ■ ++l+l108.118..132.,146—4179179i—. m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11 )tetradeca... 188

3160 31.80 32.00 32.20 5000 79 91 m/z 184.10 20.04% 55 67 131 105 117 -— Ml—.1145.159.173.. I m/z-> 10 20 30 40 50 60 70 80 90 100110120 130140150 160170180190 Abundance #79791: Benzene, 1 -(1 -cyclohexen-1 -yl)-4-methoxy- ,1d P — । 1 । । । >> । । । । 188 31 60 31.80 32.00 32.20 m/z 78.10 14.76% 5000 160

— 91 115 129 145 173 41 51 65 li, I 102 h l i HH TMTTT -----HH 4 4™ . n I 1— । । i r i > । । m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

11285.D SCAN020507.M Fri May 17 13:08:22 2002 Page 5

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