GCMS analysis results for sample AE11285, May 2002

NYC 9/11 Public Portal Document Llorary searen compound Report

Data File : C:\MSDCHEM\1\DATA\020516\11285.D Vial: 13 Acq On : 16 May 2002 9:13 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 5H-Dibenzo(a,d]cycloheptene Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.25 ug/1 19372 Phenanthrene-dl0 31.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5H-Dibshzo[a,d]cycloheptene 192 C15H12 000256-81-5 59 2 2-Propen-1-one, 1-(2-hydroxy-3-m... 192 C11H1203 040992-03-8 59 3 Bitoscanate 192 C8H4N2S2 004044-65-9 53 4 Bitoscanate 192 C8H4N2S2 004044-65-9 53 Abundance Scan 4767 (31.088 min): 11285.D (-4757) (-) m/z 192.10 100.00% 192

5000

70 o ML 44 146 329 30.80 31.00 31.20 31.40 m/z 146.20 11 < i > j ■ । • 1111 TImuumuOTT 16.40% ■nfz-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #80999:5H-Dibenzo[a,d]cycloheptene 192

177 5000 ■ 1 i 1 ■ ■ ■ । ' ■ ■ i > ■ ■ • i ■ ■ 30.80 31.00 31.20 31.40 m/z 191.10 16.37% 89 39 63 115 152 miz-> 6 ----- 111 17 20 1" 1 LU 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #80998:2-Propen-1-one, 1-(2-hydroxy-3-methoxy-6-methylphe... 192 fl

30.80 31.00 31.20 31.40 177 5000 m/ z 70.00 16.10% 55 77 103 131 159

n/z-> 0 II, 4 I'''' I'1'' I''1' I'''' I ■'1' I' 20 40 60 ‘1—0000011010010—1010 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #125827: Bitoscanate 1 ■ i ' 1 ■ ■ i 1 ' i 1 1 1 1 rr 1 192 30.80 31,00 31.20 31.40 m/z 193.20 14.68% 5000 134 50 75 90 160 07

Tl/Z-> 4.14,374. 1 lpl A | ■ * - 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 " i" ' 1 I 1 1 1 1 I ' ' »' > j ' । < । । ' ■ 30.80 31.00 31.20 31.40

11285.D SCAN020507.M Fri May 17 13:08:22 2002 Page 4

NYC-WTC_000024582