GCMS analysis results for sample AE08429, May 2002

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Laboratory report documenting GCMS analysis of sample AE08429 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048207–000048219

Folder label: “GCMS X 4/9/02 A 4/19/02”

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Data File : C:\MSDCHEM\l\DATA\020419\08429.D Vial: 16 Acq On : 19 Apr 2002 10:54 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 Anthracene-dlO- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.28 ug/1 605214 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 87 2 Phenanthrene-dlO 188 C14D10 001517-22-2 83 3 Benzene, 1-(1-cyclohexen-l-yl)-4... 188 C13H160 020758-60-5 42 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 36 Abundance Scan 4914 (31.951 min): 08429.D (-4908) (-) m/ z 188.20 100.00% 188

5000

80 94 "‘I i ■ ' ' 1 i ■ ' ' 1 i ■ 1 ■ ■ i ' 40 160 , । 31.60 31.80 32.00 32.20 66 132 146 ,n |j| mmmmmPTHTHT‘OOOu*uuuuuu m/ z 94.10 16.20% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 TIT 31.60 31.80 32.00 32.20 m/z 189.20 16.13% 80 94 160 , . 17 30 42 52 66 108118 132 146,4179179 — ■ i " 1 r i" 11 r "' i1" ■ i111 ----H TInpntut v m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 1(18 TTI i ' ■ ' 1 i 1 1 ' 1 I ' 1 1 1 I 1 31.60 31.80 32.00 32.20 5000 m/z 80.10 14.30%

80 94 160 30 42 52 66 , 11 108 118 132 146 .1,1 170179,1,1 | TITTTTTTTTTTTTTHTTTHT T0 I, i | I i i | । i i rr |-| | i i | 11 | I I | i I , I i r’l’l" i i I I I I i i | I’l’lI fill n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79791: Benzene, 1 -(1 -cyclohexen-1 -yl)-4-methoxy- 188 31.60 31.80 32.00 32.20 m/z 184.05 14.02% 5000 160

91 115 129 145 173 77

n/z—> 41 51 ' i11" i TTrM । ‘ rm 11 lrrUM— 65 I 102 1 +l+ TTTTTNTT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Hr ‘lit i ■ ' ' 1 i ■ ' ' ' i ' 1 ■ ■ i ■ 31.60 31.80 32.00 32.20

08429.D SCAN020418.M Thu May 02 15:38:06 2002 Page 7

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GCMS analysis results for sample AE08431, May 2002 · Box DEP Box 27

NYC-WTC_000048121

Laboratory report documenting GCMS analysis of sample AE08431 conducted on May 6, 2002, including surrogate recovery data.

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