GCMS sample analysis results for unknowns, May 2002

Machine-extracted title · confidence 95%

Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10133 on May 17, 2002.

NYC-WTC_000046180–000046191

Folder label: “GCMS X 5/7/02 A 5/14/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020513\10133.D Vial: 20 Acq On : 14 May 2002 7:22 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene, 1-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.33 ug/1 36400 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 1-methyl- 192 C15H12 000610-48-0 53 2 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-1 47 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 45 4 Anthracene, 9-methyl-______________ 192 C15H12 000779-02-2 45 Abundance Scan 4767 (31.088 min): 10133.D (-4758) (-) m/z 192.10 100.00% 192

5000

96 160 ,.......J L...... i i । | r I t'l ] ) i r i | I I I I | I I

30.80 31.00 31.20 31.40 42 1 121 142 74 1, | 387 k20 yordt mmT 11 1 1 1 1111 " 111" 1 • 11 11' r " i '" i 1 r " 'i " i" i "i m/z 96.20 19.70% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #125853: Anthracene, 1 -methyl- 192

5000 1 30.80 31.00 31.20 31.40 165 m/z 193.20 17.77% 44 63 96 115 139 1 | n , I rti l 4 rp*dri rh mi l Hi ri + 1 ‘I‘‘‘‘A‘‘‘‘I‘AIh‘IASSII m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #80954: 3-(2-Methoxy-5-methylphenyl)acrylic acid 192 161

30.80 31.00 31.20 31.40 A I 1 ■ ' 1 i TIT

5000 105 m/z 160.20 17.11% 77 132

.. 51 M n rrTTTYYpT^nTFTTTTTTrTp-rriTTTTTyrTTTp^ m/z—> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 #125848: Anthracene, 9-methyl- 192 .... I ' I 1 1 ' ' 1 1 1 ' 1 30.80 31.00 31.20 31.40 m/z 191.20 12.72%

5000

96 EE V IT 39 63 115 139... 1 ■ i ■ " 111111 r1 n i1" 11" " i1111 rl ‘t 11TT i111 111 " ' i1 " 11'1'' i'111 r1 ■' i1' " i " '' i'1 " r ■' 1 i ' 1 ■ ' i 1 1 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 30.80 31.00 31.20 31.40

10133.D SCAN020507.M Wed May 15 08:28:52 2002 Page 5

NYC-WTC_000046188

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GCMS analysis results, sample AE10135, May 2002 · Box DEP Box 25

NYC-WTC_000046192

Gas chromatography-mass spectrometry analysis of sample AE10135 performed May 17, 2002, detecting unknown compounds and 2,4-DDD surrogate at 96% recovery.

1 shared topics · Same agency, volume and box · similarity 0.997