GCMS sample analysis results for unknowns, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020513\10133.D Vial: 20 Acq On : 14 May 2002 7:22 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title Method 508 GC/MS Scan Library C:\DATABASE\nist98.1 Peak Number 5 Di-n-octyl phthalate Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 40.52 0.58 ug/1 56631 Chrysene-dl2 39.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Di-n-octyl phthalate 390 C24H3804 000117-84-0 78 2 1/2-Benzenedicarboxylic acid, di . . . 390 C24H3804 027554-26-3 64 3 Bis (2-ethylhexyl) phthalate 390 C24H3804 000117-81-7 56 4 Phthalic acid, diisooctyl ester 390 C24H3804 001330-91-2 50 Abundance Scan 6372 (40.518 min): 10133.D (-6366) (-) m/z 149.10 100.00% 149 57 5000 . .............. / 4 011,

36 83 104 178 40.20 40.40 40.60 40.80 , , , ha q,11 LLL___ 243 279I 449 —j—r—r-i—r^-j— — —W-j—r—r—i—i—j—r-r— —i—j—r-T— —i—l|—r t t t t t rn/z57.20 61.18% Tn/z-> 50 100 150 200 250 300 350 400 450 Abundance #123444: Di-n-octyl phthalate 149

5000 57 LAAA,— AMA 40.20 40.40 40.60 40.80

m/z-> Abundance JU 50 83 44, li . 113

100 150 75196 200 r 250 279

#67063:1,2-Benzenedicarboxylic acid, diisooctyl ester 300 350 400 450 m/z 70.10 39.53%

149 1AAA...... 1 1 1' 1 1 1 1 ' 1 40.20 40.40 40.60 40.80 5000 m/z 167.00 29.55% 57

28 I 83104 279 — ,ll1 .I1.1 T LA 1 1 1 1 1 ■ 1 ' ........................ I ' i 1 1 1 ' 1 1 1 1 ______________________ ' i ■ ■ r r I ' 1 1 1 1 1 1 1 1 1 1 n/z—> 50 100 150 200 250 300 350 400 450 Abundance #66784: Bis(2-ethylhexyl) phthalate .............. I AA........... 1 1 I ' । । | I । i i | | i r i । 1 i i > । 149 40.20 40.40 40.60 40.80 m/z 71.20 26.60% 5000 57

11.83. 113 AJ I 279 AA /z—> 50 100 150 200 250 300 350 400 450 40.20 40.40 40.60 40.80

10133.D SCAN020507 .M Wed May 15 08:28:53 2002 Page 7

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