GCMS analysis page for sample AE11570, May 2002

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Data File : C:\MSDCHEM\1\DATA\020521\11570.D Vial: 23 Acq On : 22 May 2002 6:05 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Thiazole, 2-(phenylthio)- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.26 ug/1 25343 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Thiazole, 2-(phenylthio) - 193 C9H7NS2 033342-67-5 38 2 3-Amin>-7-methyl-l,2,4-benzotria. . . 192 C8H8N4O2 1000213-87-8 38 3 p-Meth xy- .alpha.-methyl-cinnami... 192 C11H1203 1000227-16-5 38 4 Thioph ne. 2-[2-(3-thienyl)ethen. .. 192 C10H8S2 116854-09-2 38 Abundance Scan 4768 (31.094 min): 11570.D (-4760) (-) m/z 192.10 100.00% 192

5000 146 A

u42L—p66 IIIr7 90 120, h II —, 484 30.80 31.00 31.20 31.40 0- i m/z 146.20 29.59% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #81050: Thiazole, 2-(phenylthio)- 192

5000 30.80 31.00 31.20 31.40 58 m/z 191.20 17.85% 1091 148 01 I 11 . i IB 1 111 miz-> 50 100 150 200 250 300 350 400 450 Abundance #80865:3-Amino-7-methyl-1,2,4-benzotriazine 1,4-dioxide 192 L 30.80 31.00 31.20 31.40 5000 m/z 160.20 13.72% 65 150 89 42 , , , 121 01 / A I, J .1 — 11............. ....................... ■ n/z-> 50 100 150 200 250 300 350 400 450 Abundance #80851: p-Methoxy-.alpha.-methyl-cinnamic acid T * 1 ‘ 1 ' ' I • ' । I ’-| 1 1 I 1 1 192 30.80 31.00 31.20 31.40 m/z 193.10 12.31% 5000 45 77 115 147

0 J L L 4 l, I 1 I . 1 Tl/Z-> 50 100 150 200 250 300 350 400 450 30.80 31.00 31.20 31.40

11570.D SCAN020521.M Fri May 24 09:48:55 2002 Page 4

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