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Document fragment from DEP Box 27, April 2002

Machine-extracted title · confidence 80%

Single page document fragment from the DEP Box 27 archive folder dated between April 10 and April 15, 2002.

NYC-WTC_000048683–000048692

Folder label: “GCMS X 4/10/02 A 4/20/02

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Scanned page image, NYC-WTC_000048690
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020419\08489.D Vial: 26 Acq On : 20 Apr 2002 8:45 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Thiocyanic acid, 2-benzothi... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.32 ug/1 652135 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 50 2 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 42 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 36 4 Anthracene, 9-methyl- 192 C15H12 000779-02-2 36 Abundance Scan 4767 (31.088 min): 08489.D (-4760) (-) m/z 192.10 100.00% 19 2

5000 40*

96 ......................... ..................

miz-> 11 ■ •1 ■ i ‘11 • +17HmmmlmHmmmmmmmlh—r — 82

20 30 40 50 60 70 80 90 100110120130 140150 160 170180190 200 146 160 । m/z 30.80 31,00 31.20 31.40 40.10 44.54% Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 1912

5000 30.80 31.00 31.20 31.40 m/z 96.0,0 22.34% 45 7.,9, 198 122 124 148 160 iz—> 20 30 40 SO 60 70 BP 90 100110 120 130 140 ISO IS0170 180190 200 Abundance #80950: 1,5-Naphthalenedithiole 1912 ..A 30.80 31,00 31.20 31.40 5000 m/z 191.10 14.43% 115 128 159 147

m/z-> :20 30 40 50 60 70 80 90 100110120130140 150160170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 1912 30.80 31.00 31.20 31.40 m/z 193.10 10.67% 5000

96 185 f 29 39 51 > 11163 । •74"Tr (T TI 111 < 1111 T| i 11 i 83rlj ’a i j 11 j 1115 j 126 139 152 0 176 |I *11 r j 11' 1 ri-1 j 111111111 ’| 11 j i |*i i r I’t’i 11 riT j j t ***‘1484 I1 1 1 1 I 1 1 m/z—> 20 30 40 50 60 70 80 90 100 110120 130 140150 160170 180190 200 30.80 31.00 31.20 31.40

08489.D SCAN020418.M Thu May 02 12:03:59 2002 Page 4

NYC-WTC_000048690

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NYC-WTC_000048690Source: NYC Law Department, mirrored locally

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