GCMS blank results for volatile organics, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\0409LB.D Vial: 4 Acq On : 17 Apr 2002 11:51 am Operator: Nefliu Sample : 04/09 1b Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 11 Dibutyl phthalate Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

31.46 0.94 ug/L 953430 Chrysene-dl2 30.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dibutyl phthalate 278 C16H2204 000084-74-2 47 2 Benzene, l-isothiocyanato-2-methyl- 149 C8H7NS 000614-69-7 47 3 1,2-Benzenedicarboxylic acid, bu... 334 C20H30O4 000085-69-8 47 4 Didodecyl phthalate 502 C32H5404 002432-90-8 43

A Abundance Scan 4831 (31 464 min) 0409LB.D (-4820) (-) m/z 149.00 100.00% 149

5000 57 227 41 167 71 112 0— AL’— 1' j ■1 ■ ■ । ■111111' ■ । 207 , 240 279 ■1' ।■ ■ i ■ ■ ■ ■ ।1 ■ ■ ■ ।' • m/z 31.20 31.40 57.10 31.60 31.80 31.12%

M, /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #123426: Dibutyl phthalate 149

5000 TT 31.20 31.40 31.60 31.80

29 41 m/z 227.20 30.51%

n/z-> 0< 15,14 77692 704,121135. 1 167179 193295 223236 250 20 40 60 80 100 120 140 160 180 200 220 240 260 278 280 Abundance #66916: Benzene, 1-iSothiocyanato-2-methyl- 149 k........ 1 ' i ■ 1 I ‘ ‘‘I’’ 31.20 31 40 31.60 31 80 5000 m/z 167.00 18.38% 117 91

n/z-> Abundance 01 m 4J 20 40 51 1 77 60 133 80 100 120 140 160 180 200 220 240 k... #123457: 1,2-Benzenedicarboxylic acid, butyl 2-ethylhexyl ... 260 280 A.MM4.A,. 149 31.20 31 40 31.60 31.80 m/z 41.05 16.12% 5000

0 ........... 41 Il 57 70 L 112 132 167 205 223 „MWA/wd ■ • l ■ ■ ■ ■ i ■ TIT ir^ /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 31.20 31.40 31 60 31.80

0409LB.D 041702SCAN.M Thu Apr 18 09:42:01 2002 Page 18

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