Water quality monitoring data sheet, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051302\11311.D Vial: 13 Acq On : 13 May 2002 9:36 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 5/10/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L

Peak Number 15 Dibutyl phthalate Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

24.69 0.12 ug/L 126973 Phenanthrene d-10 22.53

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Dibutyl phthalate 278 C16H2204 000084-74-2 86 2 Dibutyl phthalate 278 C16H2204 000084-74-2 83 3 1,2-Benzenedicarboxylic acid, bu... 334 C20H30O4 000085-69-8 80 4 1,2-Benzenedicarboxylic acid, di... 278 C16H2204 000084-74-2 78 Abundance Scan 1501 (24.690 min): 11311.D (-) m/z 149.10 100.00% 149

5000

TImunom 57 71 85 104 13 24.40 24.60 24.80 25.00 205 223 oW ndjemhhp Iley, msiiyon L■ i 169 1 1 m/z 57.00 10.63%

1 ■ ■ ’ ■ i■•■'i • ■ ■ ■ I' • ‘' 1 ■ ■ ■ ■ i ■■■•i ■ m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223244: Dibutyl phthalate 149

5000 M24.40 24.60 24.80 25.00 m/z 150.10 9.18% 41 | 57 76 104 121

m/z-> 0 —404 ■' r1 1 274 205 223 1. i 11 ■ • ■ i ■ ■'111 ■ ■' i ■ ■ ■ ■ i' ■ ■' i' ■ ■' i ■ ■ ■ ■ i ■ 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223247: Dibutyl phthalate 149

24.40 24.60 24.80 25.66 5000 m/z 104.00 6.84%

104 205 223 |, 122 278 0 11’111102100TTB’281013311—1 1CT—1 31B—O333"73318 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #284878:1.2-Benzenedicarboxylicacid, butyl 2-ethylhexyl... 149 24.40 24.60 24.80 25.66 m/z 85.10 6.35%

W 5000

41 I 56 76 104 101 m/z-> 0 —440 4121135. 165179 1 205 223 267 ■ I ■ ■ ■ ■ i ■ ■ " i ■" ■ u 1 ■ ■ i ■ ■ " i ■' ■' i ■ 60 80 100 120 140 160 180 200 220 240 260 280 24.40 24:60 24.80 25.00

1311.D 050802.M Tue May 14 11:10:46 2002 Page 17

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