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Laboratory blank analysis results, sample AE11755, May 2002

Machine-extracted title · confidence 90%

Blank analysis for sample AE11755 to verify absence of contamination in laboratory equipment and procedures, completed May 13, 2002.

NYC-WTC_000016024–000016054

Folder label: “525 X 5/10/02 A 5/13/02

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Scanned page image, NYC-WTC_000016046
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051302\LBA0513.D Vial: 8 • Acq On : 13 May 2002 5:46 pm Operator: Bohlk / Inst 213 Sample : LB 5/10/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L

Peak Number 13 1,2-Benzenedicarboxylic aci... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

24.69 0.14 ug/L 110448 Phenanthrene d-10 22.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, bu... 362 C22H3404 000089-18-9 64 2 Dibutyl phthalate 278 C16H2204 000084-74-2 53 3 1,2-Benzenedicarboxylic acid, bu... 362 C22H3404 000089-19-0 53 4 1,2-Benzenedicarboxylic acid, di... 278 C16H2204 000084-74-2 53 Abundance Scan 1501 (24.690 min): LBA0513.D (-) m/z 149.00 100.00% 14.9 '

5000

— 57.85 113 24'46 24'66 24.80 25.66 0- ",4,h pl, 1 । 205 t 1 • • i • • m/z 57.10 13.05% miz-> 50 100 150 200 250 300 350 Abundance #308007:1,2-Benzenedlcarboxyllc acid, butyl 8-methylnonyl... 149

5000 NMdMw 24.40 24.60 24.80 25.00 m/z85.00 9.88% 41 . 223 0- 1 . ", "116.194125 176 t 1 ________ 307 trer t$ " i r ' I ‘ > 1 l > , ‘ 1 1 1 > i , I > । m/z-> 50 100 150 200 250 300 350

Mulk Abundance #223237: Dibutyl phthalate 149

24.40 24.60 24'66 25.66 5000 m/z 150.00 9.05%

41 0- 1. .76 194mT129 , ‘ [ * ■ I r 1 178 205225 r I f | I I I | I I ! | 278 miz-> 50 100 150 200 250 300 350 Abundance #308006:1,2-Benzenedlcarboxyllc acid, butyl decyl ester $... 149 24.40 24'60 24.80 25.66 m/z71.20 9.02%

5000

aheakqlMac 41 223 0 15,| , 176.97, 121 176 1, 1 307 363 1 1 ■ m/z-> 50 100 150 200 250 300 350 24.40 24.60 24.80 25.00

BA0513.D 050802.M Tue May 14 10:36:18 2002 Page 15

NYC-WTC_000016046

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NYC-WTC_000016046Source: NYC Law Department, mirrored locally

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