GCMS blank results for volatile organics, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\0409LB.D Vial: 4 Acq On : 17 Apr 2002 11:51 am Operator: Nefliu Sample : 04/09 1b Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 12 IH-Azonine, octahydro­ Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T. 34.34 0.59 ug/L 510438 Perylene-dl2 34.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 lH-Azonine, octahydro- 127 C8H17N 005661-71-2 2 2 Tridecylamine 199 C13H29N 002869-34-3 1 3 IH-Azonine, octahydro- 127 C8H17N 005661-71-2 1 4 Dexpanthenol 205 C9H19N04 000081-13-0 1 Abundance Scan 5320 (34 337 min) 0409LB.D (-5315) (-) m/z 40.00 100.00% 4b

5000

133 180 207 76 98 i ■ ■ ■ ■ i 34 00 34.20 34.40 34.60 i ■ ■ ■ ■ i

O—TT LI I I I 57 I’’’ ’I I I 281 m/z 207.00 19.28%

__N n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #108185. 1H-Azonine. octahydro- 3) 43 56

70 5000 i ■ ■ ■ 1 i

127 34 00 34.20 34 40 34 60 84 96 m/z 207.90 19.12% 15 112 0- H ------- m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #726: Tridecylamine 3b aa/aadyznsappddaas—akpyayonponMonn— 34.00 34.20 34.40 34.60 5000 m/z 41.10 18.63%

m/z-> 18 I 43 55 69 J L L 83 100 114 128 142 156 170 184 199 0- - " , " , T i h , H, , " ,, 11, 1..’. , । ~ ‘ I. 20 40 60 80 100 120 140 160 180 200 220 240 260 280 aclurho" Abundance #744: 1H-Azonine, octahydro- I 1 ' ' 1 1 3) 43 .56 34 00 34.20 34.40 34.60 m/z 150.0017.89% 70

manitkr—ah 5000 84 127 M 98

m/z—> 0 — 15 20 —u.4 1 I 40 60 80 100 112 --------------- 120 140 160 180 200 220 240 260 280 34.00 34 20 34 40 34 60

0409LB.D 041702SCAN.M Thu Apr 18 09:42:01 2002 Page 19

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