GCMS Analysis Results, Sample AE08261, April 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\08261.D Vial: 18 Acq On : 17 Apr 2002 11:29 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 Acetic acid, 2-(1-buten-3-y. .. Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 34.04 0.39 ug/L 511667 Perylene-dl2 34.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 2-(l-buten-3-yl) -2-... 187 C8H13NO4 1000159-10-0 9 2 2-Pyrrolidinethione 101 C4H7NS 002295-35-4 9 3 Azocine, octahydro- 113 C7H15N 001121-92-2 5 4 Propanal, 2,2-dimethyl-, oxime______ 101 C5H11NO 000637-91-2 4 Abundance Scan 5269 (34 038 min) 08261 D (-5268) (-) m/z 40.00 100.00% 40

5000

• 56 71 95 — 86 r 113 137 207 33.80 34 00 34.20 34.40

n/z—> 0+ L 40 60 80 100 120 1 140 160 180 200 m/z71.00 27.59% Abundance #394' Acetic acid, 2-( 1-buten-3-yl)-2-nitro-, ethyl ester . 29

5000 41 55 1 1 1 I 1 ' 1 1 I 10mppmp 4 ।, 69 33.80 34.00 34 20 34.40 83 95 112 m/z73.00 25.45% 0+ ' 1 1 1 11 1 I L dililiLi,. .,1.11111,1., +il——— 1 1 1 1 126 140 157 170 1 1 t"*r 1 1 1“' 1 1 ' I 1 1 1 ' I Immmmmni n/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #108420 2-Pyrrolidinethione 4) 101 33.80 34.00 34.20 34.40 5000 m/z 86.00 23.54% 60 73

n/z- > 0+ 20 40 Jzlalll86 60 80 III, 100 120 140 160 180 200 Abundance 39 56 #814 Azocine, octahydro- ' 1 i ■ ‘ ill— 33.80 34.00 34 20 34.40 70 m/ z 72.00 20.50% 43 5000 113 84

Tl/Z--> 0 15 1 41i20 1 1 —l 40 I . i|l I ...ii । 98 .1 11 n , । । , TI । । । "| । । i" । । । । 60 80 100 120 140 160 180 200 ■ ■ i ■ ■ ' ' 1 1 ' ' 1 I ' 1 33 80 34 00 34.20 34 40

08261.D 041702SCAN.M Thu Apr 18 09:47:24 2002 Page 16

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