GCMS Analysis Results, Sample AE08261, April 22, 2002

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Library Search Compound Report Data File C:\MSDCHEM\l\DATA\020417\08261.D Vial: 18 Acq On 17 Apr 2002 11:29 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 Decanedioic acid, bis(2-eth... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 33.93 2.82 ug/L 3665450 Perylene-dl2 34.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Decanedioic acid, bis(2-ethylhex... 426 C26H50O4 000122-62-3 72 2 1,2,4-Triazolo[4,3-a]pyridine-3(... 185 C6H4C1N3S 022841-91-4 38 3 [1,1' -Biphenyl] -4-ol, 3-amino- 185 C12H11NO 001134-36-7 32 4 dl-2-Ethylhexyl chloroformate 192 C9H17C1O2 024468-13-1 30 Abundance Scan 5250 (33.926 min): 08261 D (-5240) (-) m/z 185.10 100.00% 185

57 5000- ■ 112 83 I ■ ' I ' ' ’ ' I 1 ' ' 1 I ' ‘ ' I TIT

n/z-> 0- 116.50 100 150 203 —— — 200 250 268 297315 300 350 400 33 60 33 80 m/z57.10 34.00 34 20 52.69% Abundance #78968: Decanedioic acid, bis(2-ethylhexyl) ester 185

57 5000 112 112007 33.60 33.80 34.00 34.20 m/z 70.10 33.77% —4 L+ 83 297315 29 । I 143 166 203 0- +44144 , । 227 | 255 279 1 I 340 370 397 426 n/z- > 50 100 150 200 250 300 350 400 Abundance #79124: 1,2,4-Triazolo[4,3-a]pyridine-3(2H)-thione, 8-chloro- 185 l 1 ' H 33 60 -33 80 34.00 34.20 5000- m/z71.10 32.70% 127 64 92 of . .,1 L L. I v 1158 41 । , 4 I 1 Tl/Z--> 50 100 150 200 250 300 350 400 Abundance #79028: [1,1 ‘-Bipheny!]-4-ol, 3-amino- 185 I 1 ' ' ' I 1 33.60 33.80 34 00 34.20 m/z 112.10 28.61% 5000-

156

n/z— > 0 27.517522 2LL 200 50 100 150 250 300 350 400 — ———m———e04T 33.60 33.80 34.00 34 20

08261.D 041702SCAN.M Thu Apr 18 09:47:24 2002 Page 15

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