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GCMS blank results for volatile organics, April 2002

Machine-extracted title · confidence 100%

Laboratory report showing blank analysis results for volatile organic compounds in sample AE08260 from April 2002.

NYC-WTC_000048225–000048255

Folder label: “GCMS X 4/9/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020417\0409LB.D vial: 4 Acq On 17 Apr 2002 11:51 am Operator: Nefliu Sample 04/09 1b Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 1,2-Benzenedicarboxylic aci... Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

34.70 0.87 ug/L 742553 Perylene-dl2 34.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, di . . . 446 C28H4604 026761-40-0 9 2 1,2-Benzenedicarboxylic acid, is... 418 C26H4204 001330-96-7 9 3 Di-n-octyl phthalate 390 C24H3804 000117-84-0 9 4 Decane, 2,3,6-trimethyl- 184 C13H28 062238-12-4 9 Abundance Scan 5382 (34 702 min) 0409LB.D (-5371) (-) m/z 149.00 100.00%

5000 40 149

WAARH WW* 69 81 99 207 307 167 34.40 34 60 34.80 35.00

n/z-> 0—T —IT 20 40 511 JU ........... ... 80 100 120 140 160 180 200 220 240 260 280 300 60 m/ z 40.00 88.68% Abundance #66777: 1,2-Benzenedicarboxylic acid, diisodecyl ester 149

5000- 43 57 71 85 34.40 34.60 34.80 35.00 m/z 43.1054.39% 167 —440 41241s+ MAe/y 29 307 0 TI m/z-> 20 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #67006: 1,2-Benzenedicarboxylic acid, isodecyl octyl ester 149 AAMM । ' I r< । i |-|->r > । > < > ■ । 34.40 34 60 34.80 35.00 5000 m/z 69.00 37.64%

/z— > Abundance 20 4 3 5 7 71 84 104 123 29 1 J irrti 0V........ ‘ T+r111 20 40 60 80 100 120 140 167 160 180 200 220 240 260 280 300 #123450 Di-n-octyl phthalate 261 279 307 sM*/h 149 34.40 34.60 34.80 35.00 m/z 57.10 35.80%

5000 „MA“tw 29 43 57 71 261 279 ppsa-“r"" 84 104 123 0 — TTTt 167 i 1 ■ ■ 1 i ' ■ ■ ■ i' 1 1 11 1 1 '' I । I i

Ti/Z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 34.40 34.60 34 80 35.00

0409LB.D 041702SCAN.M Thu Apr 18 09:42:03 2002 Page 21

NYC-WTC_000048248

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NYC-WTC_000048248Source: NYC Law Department, mirrored locally

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