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GCMS reference analysis results for volatile organics, June 2002

Machine-extracted title · confidence 90%

Laboratory report listing reference values for volatile organic compounds in sample AE12735 with associated numerical data.

NYC-WTC_000015171–000015199

Folder label: “GCMS X 6/3/02 A 6/7/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\060702\12735.D Vial: 11 Acq On 7 Jun 2002 4:43 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 19 1,2-Benzenedicarboxylic aci... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 25.05 1.00 ug/L 1081210 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qi 1 1,2-Benzenedicarboxylic acid, bu... 304 C18H24O4 000084-64-0 90 2 Dibutyl phthalate 278 C16H2204 000084-74-2 (83 3 Dibutyl phthalate 278 C16H2204 000084-74-2 83 4 1,2-Benzenedicarboxylic acid, bi... 278 C16H2204 000084-69-5 78 Abundance Scan 3739 (25.048 min): 12735.D (-3731) (-) m/z 149.00 100.00% 149

5000

...... ........ . ,, 24.80 25.00 25.20 25.40

miz-> 0 :20 —415776 —494122135, .... 205.223 ..... 40 60 80 100 120 140 160 180 200 220 240 260 280 m/z 150.00 8.79% Abundance #66736:1,2-Benzenedicarboxylic acid, butyl cyclohexyl ester 149

5000 24.80 25.00 25.20 25.40 m/z 41.10 7.68% 0- , ? 1 5 %7 ,83.1.194, 121 135 . ;167 205 223 T m/z—> 20 40 60 80 100 120 140 160 180 - 200 220 240 260 280 Abundance #123447: Dibutyl phthalate 149 24.80 25.00 25.20 25.40 5000 •m/z 104.00 4.74%

57 76 104 205 223 0 - T 122 11 278 miz-> :20 40 60 80 '100 120 140 160 180 200 220 240 260 280 Abundance #123432: Dibutyl phthalate 149 24.80 25.00 25.20 25.40 m/z 57.10 4.18% 5000

157 76 104 121 /z—> O-TT .. n 11 । ‘ 0p .1900274 20 40 60 80 100 120 140 160 180 200 220 240 260 280 24.80 25.00 25.20 25.40

12735.D 060302.M Mon Jun 10 11:22:58 2002 Page 22

NYC-WTC_000015197

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NYC-WTC_000015197Source: NYC Law Department, mirrored locally

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