GCMS reference analysis results for volatile organics, June 2002

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Data File C: \MSDCHEM\1\DATA\060702\12735.D Vial: 11 Acq On 7 Jun 2002 4:43 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 18 Anthracene-dlO- Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.33 ug/L 352870 Phenant hranene - dl 0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qua 1 Anthracene-d10- 188 C14D10 001719-06-8 91 2 Phenanthrene-diO 188 C14D10 001517-22-2 78 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 42 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 40 Abundance Scan 3401 (23.062 min): 12735.D (-3394) (-) m/z 188.10 100.00% 188

5000

80 94

m/z-> 0 43 57 66 | | m 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 160 । 1’117 22.80 23.00 23.20 23.40 m/z 189.10 18.10% Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 184.00 14.24% 17 30 42 52 66 80 94 160 ,i ,, 0- I ■■ ■ ■ l ".i|i ■ ■ ■ l ■ ■ ■■ I n i TTTHmHmm I 108118 132 146 I, 170179,1 mfz-> 10 20 30 40 50 60 70 80 90 100110120 130140150160170180190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/ z 94.05 13.05%

80 94 160 30 42 52 66 11 108118 132 146 I 170179,1 0 IIUIummmmn—ut—a—mmm—uHTTTPum n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79804: Naphthalene, 1,7-dimethoxy- ) 1 173 188 22.80 23.00 23.20 23.40 m/z 8.0.10 12.26%

5000 102 115 145 51 63 75 130 158 ।

n/z—> 0 -H ... II..... 1, 1 44.... 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 pTTT 22.80 23.00 23.20 23.40

12735.D 060302.M Mon Jun 10 11:22:58 2002 Page 21

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