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GCMS analysis results for unknown compounds, June 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE12736 with surrogate recovery data and identification of unknown compounds.

NYC-WTC_000015224–000015252

Folder label: “GCMS X 6/3/02 A 6/7/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\060702\12737.D Vial: 13 Acq On 7 Jun 2002 6:21 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 19 Anthracene-dlO- Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.32 ug/L 272432 Phenanthranene-dl0 22.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 74 2 Phenanthrene-diO 188 C14D10 001517-22-2 64 < 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 40 Abundance Scan 3401 (23.062 min): 12737.D (-3395) (-) m/z 188.10 100.00% 188

5000

80 94 158 22.80 23.00 23.20 23.40

m/z-> o- mH ll++ 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160170 180 190 m/ z 80.00 1 20.33% Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 94.00 16.37% 80 94 160 , , 17 30 42 52 00 , 108118 132 146 ,|| 170179 0 TmILTTTTH TIWTTTTTHTTTTTT ‘I /z-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 .......................... ............... 22.80 23.00 23.20 23.40 5000 m/z 189.10 16.26%

80 94 160 , 30 42 52 66 . 11 108118 132 146 1I, 170179,1,1 0- IUmmmmmu—u—mHT : I ri 11 r i! 1111J111111 n i i 111 n | i it Tj i 11 111 TTTTT 11 TM i i r11 mtz-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline T_ -----I_ I_ 1_ 1 18 8 22.80 23.00 23.20 23.40 m/z 184.10 15.17% 145 5000

117

n/z-> 0 41 51 63 77 89 102 m 130 159 173 I mpj 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 I— 22.80 23.00 23.20 23.40

12737.D 060302.M Mon Jun 10 11:24:29 2002 Page 22

NYC-WTC_000015250

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NYC-WTC_000015250Source: NYC Law Department, mirrored locally

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