Laboratory report documenting GCMS analysis of sample AE12736 with surrogate recovery data and identification of unknown compounds.
NYC-WTC_000015224–000015252Folder label: “GCMS X 6/3/02 A 6/7/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document LIbrary Search Compound Report
Data File C:\MSDCHEM\l\DATA\060702\12737 .D Vial: 13 Acq On 7 Jun 2002 6:21 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 20 Nickelocene, 1,2,3,4,5-pent ... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T.
34.87 0.60 ug/L 161328 Perylene-d12 34.65
Hit# of 5 Tentative ID MW MolForm CAS# Qua
1 Nickelocene, 1,2,3,4,5-pentamethyl- 258 C15H20N1 075730-73-3 7/ 2 9,10-Anthracenedione, l-chloro-4... 258 C14H7C103 000082-42-8 5 3 l-Butyl-3-p-methylphenyl-2,4,5-t... 260 C14H16N2O3 064836-40-4/5 4 Benzene, (1 hexyl-1-heptenyl)- 258 C19H30 055030-46-1 4 Abundance Scan 5411 (34.872 min): 12737.D (-5409) (-) m/z 117.90 100.00% 1’8 208 86 33 258 44
5000
281 ---Pp- 34.60 34.80 35.00 35.20 OTT । ■1 ■ ।'' ■ ■ । ‘ । ‘।' 111 ■' ■ ■ i ■ ■ m/z 207.90 81.98% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #94313: Nickelocene, 1.2,3,4,5-pentamethyl- 258
192 5000 58 91 119133 176 m/z 129.00 41 105 150 164 81.53% 27 । 71 0- - 4+44 +444444L — 231243 । 1— 11 ■ ‘ ■ i f ■ m/z-> 20 40 60 80 100 120 140 160 180.200 220 240 260 280 Abundance #94380:9,10-Anthracenedione, 1-chloro-4-hydroxy- 21 8 TT 34.60 34.80 35.00 35.20 5000 m/z 257.90 75.68% 139 . 202 230
n/z-> 0- +50.4243191113125,4 20 153,73 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #60332:1-Butyl-3-p-methylphenyl-2,4,5-trioxoimidazolidine ■ i ■ ■ ■ ■ i ■ ■ 133 34.60 34.80 35.00 35.20 m/z 133.20 74.32%
5000 260
41 56 77 91 104 || 204 O ' i 1 1 1 1 P 11) 7 " '■ 'i । | l'i ' । । 1 1 1 1 ' 1 1 I 1 1 1 1 1 1 ----- n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34.60 34.80 35.00 35.20
12737.D 060302.M Mon Jun 10 11:24:31 2002 Page 23
NYC-WTC_000015251
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NYC-WTC_000015282
Laboratory report documenting GCMS analysis of sample AE12738 with surrogate recovery data and identification of unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015171
Laboratory report listing reference values for volatile organic compounds in sample AE12735 with associated numerical data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015696
Report documenting the recovery percentage of the 2,4-DDD surrogate standard used to validate gas chromatography-mass spectrometry analysis.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015806
Report documenting surrogate recovery for sample AE12763 analyzed on June 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013049
Laboratory report showing blank sample analysis for volatile organic compounds using gas chromatography-mass spectrometry on May 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013496
Laboratory report documenting GCMS analysis of sample AE11928 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012989
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012852
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11901.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012908
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015536
Gas chromatography-mass spectrometry analysis report for sample AE12765 detecting unknown compounds and surrogates on June 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044025
Laboratory report for sample AE09973 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043893
Laboratory report for sample AE09771 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000015131
Department of Environmental Protection record of GCMS results generated in early June 2002.
Filed in the same folder
NYC-WTC_000015132
Partial text fragment from a Department of Environmental Protection record dated between June 3 and June 7, 2002.
Filed in the same folder
NYC-WTC_000015135
Log sheet recording sample numbers, drip rates, pH levels, and other processing metrics for multiple environmental samples.
Filed in the same folder
NYC-WTC_000015159
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank sample AE12735.
Filed in the same folder
NYC-WTC_000015163
Laboratory report displaying calibration percentages for various volatile organic compounds including nitrosamines and chlorobenzenes.
Filed in the same folder