GCMS analysis results for unknown compounds, sample AE10202, May 2002

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Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10202 on May 10, 2002.

NYC-WTC_000045020–000045044

Folder label: “GCMS X 4/30/02 A 5/8/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\10202 .D Vial : 20 Acq On 9 May 2002 6:53 am Operator: Me lean Sample 4/30 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 15 1,3-Cyclopentanedione, 2-ch... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 34.92 0.23 ug/L 247437 Perylene-dl2 34.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Cyclopentanedione, 2-chloro- 132 C5H5C1O2 014203-19-1 43/ 2 Ethyl 4-(4-nitrophthalimidomethy . . . 369 C18H15N3O6 1000224-83-3/12 3 3-Propyl-benzotriazine-4-one 189 C1OH11N30 1000146-11-5 10 4 3-Pyridinecarbonitrile, 5,6-dime... 132 C8H8N2 113124-09-7 9 Abundance Scan 5420 (34.925 min): 10202.D (-5418) (-) m/z 131.70 160.00% 132

5000 96 115 209 51 262 281 34.60 34.80 35.00 35.20 0 .... |i 73 m/z 130.70 40.88% TT 111 " "I’t 1111 ■ •111111111 ’ ■ i1' 111| ‘ ...... ........... 11111111 111 i ■r ■11 mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #59720: 1,3-Cyclopentanedione, 2-chloro- 132

5000 69 Aul_ 34.60 34.80 35.00 35.20 ' 1 TA,4- |

39 m/z 95.90 29.77% h 1 89 105 0- --H 11‘‘‘11TT‘‘1111‘1111111101117T111111111010B1010100TTITT ‘71I‘S7 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #59617: Ethyl 4-(4-nitrophthalimidomethylamino)benzoate 1 A 132

103 34.60 34.80 35.00 35.20 75 5000 m/z 209.10 29.49%

51 -344LH " . ris 205 324341 389 0-

M I Mmzkssuarrtrhm > । ii i r। । i ■ ■ । i ■ i i । i i i i । i i i । । i i । i । । i i i । i i i i । i ri' i j

/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #59659: 3-Propyl-benzotriazine-4-one 132 34.60 34.80 35.00 35.20 105 m/ z 132.90 26.06% 160 5000 77 189 41

01! I I I I11! I i'''111' 111’’ 11 > 11111 ■ । > ।. । -1111.. 11111111111 ....... III I < । । । । r । । v ill । r i 1 i t 1

n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 34.60 34.80 35.00 35.20 -

10202.D 050102.M Thu May 09 13:37:41 2002 Page 19

NYC-WTC_000045043

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GCMS analysis results, sample AE09971, May 2002 · Box DEP Box 25

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