Laboratory report documenting GCMS analysis of sample AE11931 conducted on May 29, 2002.
NYC-WTC_000013574–000013602Folder label: “GCMS X 5/22/02 A 5/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\11931.D Vial: 11 Acq On : 23 May 2002 6:07 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 17 1,1,1,5,7,7,7-Heptamethyl-3... Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
35.38 2.97 ug/L 745295 Perylene-dl2 34.65
Hit# of 5 Tentative ID MW MolForm CAS# Qual l l,l,l,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 42 2 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H4406Si7 019095-23-9/37 3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 27 4 Octasiloxane, 1,1,3,3,5,5,7,7,9,... 578 C16H50O7Si8 019095-24/0 25 Abundance Scan 5497 (35.377 min): 11931 .D (-5482) (-) m/ z 73.10 100.00% 73 147 221
5000- 281 355 npaqphmnpprmyprpi /. romoomp 191 35.00 35.20 35.40 35.60 35.80
nfe-> 0- 1 44 l- I 50 1 1 i 1 ‘ 100 i --- 1 150 ‘ 200 ■ ■ i 250 300 350 +43274 400 450 m/z 147.00 72.92% Abundance #26950:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy).._ 73
5000 147 267 355 / 1 429 35.00 35.20 35.40 35.60 35.80 45 207 m/z 221.10 71.26%
0- ■ i ■ ■ ■ ■ r■ ■ ■ ‘ i ■ 1 1 1 i ■ ■ ■ ‘ I miz-> 50 100 150 200 250 300 350 400 450 Abundance #27374: Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tet... 73 35.00 35.20 35.40 35.60 35.80 5000 207 m/z 207.05 30.28%
mfc-> 0- Abundance . 45 1 ‘ 1 t 1
50 ,
73 . ,103. 100 150 133
200 281 17714 H , 2531 L , 3271 1 377399 429 1 1 ' 489 250 300 350 400 #115144: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 1 ’ 1 355
450 _un 35.00 35.20 35*40 35.'60 35.80 147 m/z 355.00 29.49% 5000 281 45 369 117 207 249 -, 0 i i * ■ i * • , I t t
iz-> 50 100 150 200 250 300 350 400 450 35.00 35.20 35.40 35.60 35.80
11931.D 052202.M Wed May 29 09:51:05 2002 Page 20
NYC-WTC_000013597
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NYC-WTC_000012908
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013496
Laboratory report documenting GCMS analysis of sample AE11928 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012852
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11901.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012937
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11904.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013524
Laboratory report documenting GCMS analysis of sample AE11929 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012989
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013154
GCMS laboratory report for sample AE09677 detecting unknown compounds and 2,4-DDD on May 23, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012823
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013014
GCMS laboratory report for sample AE11908 detecting unknown compounds and 2,4-DDD on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012881
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11902.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013643
Laboratory report documenting GCMS analysis of sample AE12162 conducted on June 5, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000013414
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NYC-WTC_000013418
Quality control document showing GCMS blank results for multiple volatile organic compounds analyzed on May 29, 2002.
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NYC-WTC_000013444
Calibration data sheet verifying instrument response for volatile organic compounds during GCMS analysis on May 29, 2002.
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NYC-WTC_000013448
Reference data sheet listing concentrations and detection limits for volatile organic compounds used in GCMS analysis on May 29, 2002.
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