NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\052302\11931.D Vial: 11
Acq On : 23 May 2002 6:07 pm Operator: Mclean
Sample : 5/22ad Inst : Instrumen
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 16 Octasiloxane, 1,1,3,3,5,5,7... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
34.32 2.62 ug/L 657604 Perylene-dl2 34.65
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Octasiloxane, 1,1,3,3,5,5,7,7,9,... 578 C16H50O7Si8 019095-24-0 38
2 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 35
3 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 27
4 Trisiloxane. 1,1,1,5,5,5-hexamet. . . 384 C12H3604Si5 003555-47-3/25
Abundance Scan 5318 (34.326 min): 11931 .D (-5304) (-) m/z 73.10 10/. 00%
73
147 221
5000 281
355 V
429
T-r-j-r-rT28 M Mi25M
34.00 34.20 34.40 34.60
191
0+ ■401 rr 117, n 1 1 1 1? 1 1 1 11 ‘ I * ‘ f I 1 .327 401 I
m/z 221.10 65.15%
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #27373: Octasiloxane, 1,1,3,3,5,57,7,9,9,11,11,13,13,15,1...
73
5000 207 M
34.00 34.20 34.40 34.60
281 m/z 147.10 64.43%
147
O 45, ..1171,1.1774/25141.3734317,371 40142% . 503 563
■ r1 ■1 ■ i ■ ■
nz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #115144: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim...
73
147 TT-p-rnr-r-f
34.00 34.20 34.40 34.60
5000 m/z 281.00 38.80%
281
45 ..... 369 .................
04 I ,
■ 1 i ' ‘
117
‘ i ■ ■ 1
207 249
m/z->
Abundance
50 100 150 200 250 300 350 400 450 500
#87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,57,7...
147 2211
550
< A Aamp MAHAAA/. WAAMmAmanr
34.00 34.20 34.40 34.60
m/z 207.00 30.32%
73
5000
191
W*wy
/z—>
0 45
' ‘'1 ■ '
50 100
LL
117
150 200
279
249 1.....................
250 300 350 400 450 500 550 34.00 34.20 34.40 34.60
11931.D 052202.M Wed May 29 09:51:05 2002 Page 19
NYC-WTC_000013596
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