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GCMS calibration data for sample AE11931, May 2002

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Laboratory report documenting GCMS analysis of sample AE11931 conducted on May 29, 2002.

NYC-WTC_000013574–000013602

Folder label: “GCMS X 5/22/02 A 5/23/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\11931.D Vial: 11 Acq On : 23 May 2002 6:07 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 16 Octasiloxane, 1,1,3,3,5,5,7... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 34.32 2.62 ug/L 657604 Perylene-dl2 34.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Octasiloxane, 1,1,3,3,5,5,7,7,9,... 578 C16H50O7Si8 019095-24-0 38 2 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 35 3 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 27 4 Trisiloxane. 1,1,1,5,5,5-hexamet. . . 384 C12H3604Si5 003555-47-3/25 Abundance Scan 5318 (34.326 min): 11931 .D (-5304) (-) m/z 73.10 10/. 00% 73 147 221 5000 281 355 V 429 T-r-j-r-rT28 M Mi25M 34.00 34.20 34.40 34.60 191 0+ ■401 rr 117, n 1 1 1 1? 1 1 1 11 ‘ I * ‘ f I 1 .327 401 I m/z 221.10 65.15% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #27373: Octasiloxane, 1,1,3,3,5,57,7,9,9,11,11,13,13,15,1... 73

5000 207 M 34.00 34.20 34.40 34.60 281 m/z 147.10 64.43% 147 O 45, ..1171,1.1774/25141.3734317,371 40142% . 503 563 ■ r1 ■1 ■ i ■ ■ nz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #115144: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 73 147 TT-p-rnr-r-f 34.00 34.20 34.40 34.60 5000 m/z 281.00 38.80% 281 45 ..... 369 ................. 04 I , ■ 1 i ' ‘ 117 ‘ i ■ ■ 1 207 249 m/z-> Abundance 50 100 150 200 250 300 350 400 450 500 #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,57,7... 147 2211 550 < A Aamp MAHAAA/. WAAMmAmanr 34.00 34.20 34.40 34.60 m/z 207.00 30.32% 73 5000 191 W*wy /z—> 0 45 ' ‘'1 ■ '

50 100 LL 117

150 200 279 249 1..................... 250 300 350 400 450 500 550 34.00 34.20 34.40 34.60

11931.D 052202.M Wed May 29 09:51:05 2002 Page 19

NYC-WTC_000013596

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NYC-WTC_000013596Source: NYC Law Department, mirrored locally

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