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GCMS Analysis Results, Sample AE08261, April 22, 2002

Machine-extracted title · confidence 100%

Initial analysis page for sample AE08261 showing surrogate recovery data and unknown compound screening.

NYC-WTC_000048287–000048308

Folder label: “GCMS X 4/9/02 A 4/17/02

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Scanned page image, NYC-WTC_000048304
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\08261.D Vial: 18 Acq On : 17 Apr 2002 11:29 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 Benzoic acid, 3-(phenylamin... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T. 31.46 0.25 ug/L 400764 Chrysene-dl2 30.89 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 3-(phenylamino)-, ... 227 C14H13NO2 055622-43-0 32 2 Benzoic acid, p-anilino-, methyl... 227 C14H13NO2 004058-18-8 32 3 Silicic acid (H6-Si2-07), hexame... 258 C6H1807Si2 004371-91-9 23 4 1,2-Benzenedicarboxylic acid, mo.. 278 C16H2204 004376-20-9 10 Abundance Scan 4830 (31.458 min): 08261 D (-4820) (-) m/z 227.20 100.00% 2; 7

149 5000 113 167 41 57 70

n/z-> 01 .. I,III,.. I,I,..Il, 40 60 — 80 100 120 1 ^ “

140 ,......... I 160 180 200 198 —l 220 240 ’ 240 ’ 31.20 31 40 31 60 31.80 m/ z 149.00 58.30% Abundance #89078: Benzoic acid, 3-(phenylamino)-, methyl ester 227

5000 167 31 20 31.40 31 60 31 80 m/z 113.50 29.81% 196 52 66 77 89 98 115 139 I 182 |. 01 -------------- n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #89099' Benzoic acid, p-anilino-, methyl ester 227 196 31 20 31 40 31 60 31 80 5000 m/z 167.00 21.60% 167 , 77 98 41 51 65 |7 89 | 115 128 139 180 .... 01 .* "I T | V ■ ", ■ I | 1 ! “I . | I .‘ri 'I > I 'I' ' I I 'I I m/z—> 40 60 80 100 120 140 160 200 180 220 240 Abundance #89125 Silicic acid (H6-Si2-07), hexamethyl ester 2.7 31.20 31 40 31 60 31 80 m/ z 228.10 17.56% 197 5000 167 91 107 121 137 151 181 0 ,45,,,61.771 ,11 1, + ■ 1, I., * ■ — I, 213 ■ I 1 ' ■ • I ' ' • ’ I 1 ' ' ‘I ' 1 ' "r 1 I 1 1 n/Z-> 40 60 80 100 120 140 160 180 200 220 240 31 20 31.40 31.60 31.80

08261.D 041702SCAN.M Thu Apr 18 09:47:23 2002 Page 14

NYC-WTC_000048304

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NYC-WTC_000048304Source: NYC Law Department, mirrored locally

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