GCMS analysis results for sample AE08431, May 2002

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Laboratory report documenting GCMS analysis of sample AE08431 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048121–000048133

Folder label: “GCMS X 4/9/02 A 4/19/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020419\08431 .D Vial: 18 Acq On : 20 Apr 2002 12:52 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 6 Benzoic acid, p-anilino-, m.. Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 40.44 0.22 ug/1 408946 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, p-anilino-, methyl... 227 C14H13NO2 004058-18-8 47 2 Benzoic acid, 3-(phenylamino)-, ... 227 C14H13NO2 055622-43-0 40 3 5-Cyano-2-methyl-6-phenyl-4-thio... 227 C12H9N3S 013996-07-1 33 4 5-Cyano-8-dimethylamino-6-methox... 227 C13H13N3O 1000213-20-5 9 Abundance Scan 6358 (40.436 min): 08431 .D (-6353) (-) m/z 227.15 100.00% Z!7

5000 40 113 71 85 99 | 198208 it 40.20 40.40 40.60 40.80 - " | " ' | |'| " I | ' i' 1 | 1 I M I . I , | 'll > I | I I | I | | I | । | I । | । | I | I I 11 | I ITT n | I I I I 11 I iHp rl | I । I i |‘I n r m/z 40.10 27.50% mz-> 40 50 60 70 80 90 100110120130140150160170180190200210220230 Abundance #89099: Benzoic acid, p-anilino-, methyl ester Z!7 196

5000 40.20 40.40 40.60 40.80 167 m/z 228.20 19.13% 77 98 41 51 65 " " i' reppiguv — ,89 | 115 128 139 ........ u»)VW—"aTI—B—"I-I—BU*713 . i" " r ■111 ■ > ’' । > 11111 I............ ■ r "11111 ■ i • 'r' ‘' mfe-> 40 50 60 70 80 90 100110120130140150160170180190200210220230 Abundance #89078: Benzoic acid, 3-(phenylamino)-, methyl ester 27 k 40.20 40.40 40.60 40.80 5000 m/z 113.40 18.61% 167 196 " " | ' 1 . ' 52 66 7 89 98 115 139 h I ■ | > I I ! | !> I I | I I I I | > I I I | I > I I | I I I I | I I I I | 1 > I .'|............ U .... I II .182 |.............

4 Y..... , " r 1,11" " I''" i"111''1'i'''' i' m/z—> 40 50 60 70 80 90 100110120130140150160170180190200210220230 Abundance #89096: 5-Cyano-2-methyl-6-phenyl-4-thioxo-3,4-dihydropyri... Z!7 40.20 40.40 40.60 40.80 186 rn/z 113.80 17.82%

5000

153 77 i 100 127 ““TPTTTTIIIOTu ’ 1 I I. r qr. I 1 | I I < I | I I < f | I r l ।।।i" i • • 142 1...... , TTTTT 1 1 I 1 ' A*mmm ■n/z-> 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 230 40.20 40.40 40.60 40.80

08431.D SCAN020418.M Thu May 02 15:40:32 2002 Page 8

NYC-WTC_000048132

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GCMS analysis results for sample AE08426, May 2002 · Box DEP Box 27

NYC-WTC_000048169

Laboratory report documenting GCMS analysis of sample AE08426 conducted on May 6, 2002, including surrogate recovery data.

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