GCMS analysis results for sample AE08324, May 2002

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Laboratory report documenting GCMS analysis of sample AE08324 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048134–000048147

Folder label: “GCMS X 4/9/02 A 4/19/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020419\08324.D Vial: 11 Acq On : 19 Apr 2002 5:58 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 7 6-Nitro-2-methylpyrrolo[2,3... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

40.44 0.21 ug/1 397505 Chrysene-dl2 39.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 6-Nitro-2-methylpyrrolo[2,3-g]qu... 227 C12H9N302 1000071-35-1 43 2 Benzoic acid, 3-(phenylamino)-, ... 227 C14H13NO2 055622-43-0 9 3 Benzenemethanol, 3-(dimethylamin... 227 C15H17NO 086997-96-8 9 4 Phenol, 4-[[(4-methoxyphenyl)met... 227 C14H13NO2 003230-39-5 7 Abundance Scan 6359 (40.442 min): 08324.D (-6349) (-) m/z 227.20 100.00% 227

40 5000

99 113 X '— ■ 198 ,_______ L। 40.20 40.40 40.60 40.80

m/z-> — ■+-T-T 40 57.71,85,4 60 80 100 120 ■i ।_____________________________________ > ti 1 1 ■ i 1 ■ 1 1 l 1 ' 1 1 1 1 1 1 1 i 1 1 1 1 I 1 1 1 1 1 1 140 160 180 200 220 m/ z 40.10 49.23% Abundance #89088: 6-Nitro-2-methylpyrrolo[2,3-g]quinoline 227

5000 181 43 40.20 40.40 40.60 40.80 57 m/Z 113.60 24.00% |. 69 93 154 , , Il I I 83 97 ■ ■ i 1 ' 1 1 i ■ ■ 1 1 i 1 ■ 1 ' i 1 1 ' ■ i ■ ■ ■ ■ i 1 1 1 | 169 1 i 1 r 1 1 1 1 197 4 m/z-> 40 60 80 100 120 140 160 180 200 220 Abundance #89078: Benzoic acid, 3-(phenylamino)-, methyl ester 227 N 40.20 40.40 40.60 40.80 5000 m/z 22 6.10 19.80% 167 196 52 66 7 98 115 139 ■ 1 । ■ 1 1 i 1'1 ■ 1 । 1 1 1 mi ■ । । । ■■ । । 'i' । । , , , I. , 182 |... ■n/z~> 40 60 80 100 120 140 160 180 200 220 .... ............ .)...................... Abundance #89061: Benzenemethanol, 3-(dimethylamino)-.alpha.-phenyl- 227 40.20 40.40 40.60 40.80 m/z 228.10 12.38% A 5000 122 77 105 211 32,4252,65 1 11 i ■ — — 91 132 148, 12 1 1 1 1 I 1 1 1 1 1 11 181 I ■ 1 ( . . 194 | Bin ! , 'l I”| • I A n/z—> 40 60 80 100 120 140 160 180 200 220 40.20 40.40 40.60 40.80

08324.D SCAN020418 .M Fri May 03 09:04:40 2002 Page 9

NYC-WTC_000048146

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GCMS analysis results for sample AE08323, May 2002 · Box DEP Box 27

NYC-WTC_000048106

Laboratory report documenting GCMS analysis of sample AE08323 conducted on May 6, 2002, including surrogate recovery data.

1 shared topics · Same agency, volume and box · similarity 0.998