GCMS analysis results for sample AE08428, May 2002

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Laboratory report documenting GCMS analysis of sample AE08428 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048195–000048206

Folder label: “GCMS X 4/9/02 A 4/19/02”

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Data File : C:\MSDCHEM\1\DATA\020419\08428.D Vial: 15 Acq On : 19 Apr 2002 9:55 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 5 5-Cyano-8-dimethylamino-6-m... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 40.44 0.20 ug/1 416050 Chrysene-dl2 39.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5-Cyano-8-dimethylamino-6-methox... 227 C13H13N3O 1000213-20-5 33 2 2-Fluoro-4-methyl-10H-acridin-9-one 227 C14H10FNO 1000210-25-9 33 3 Benzoic acid, p-anilino-, methyl... 227 C14H13NO2 004058-18-8 28 4 1,3,5-Triazine-2,4-diamine, N-et... 227 C9H17N5S 000834-12-8 9 Abundance Scan 6359 (40.442 min): 08428. D (-6346) (-) m/z 227.20 100.00% 2.7

5000 113 40 ‘I ' । । । । 1 1 40.20 40.40 40.60 40.80 51 „ PR 74 oo 99 j u . I "14_ - । i-1 । i r i । । । 197207, , , 1 240 T-r-r-T-T m/ Z 113.60 29.10% m/z-> 40 60 80 100 120 140 160 200 180 220 240 Abundance #89117: 5-Cyano-8-dimethylamino-6-methoxyquinoline 2.7 212 .............. /...................... 5000 40.20 40.40 40.60 40.80 198 m/z 228.20 22.48% 42,52 63 76 88 101 114 127 141 155 169 184 | 1'1 |" 1 -i' r'"11 . ........... .. .. .. i ............................ . ■ ■ 1 । । m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #89104: 2-Fluoro-4-methyl-1 OH-acridin-9-one 227 A ■ 1 i ■ ' • ■ i ■ ' 40.20 40.40 40.60 40.80 5000 m/z 40.10 22.21% 198

13,57,67, 7789,9% 113 125 140 151, 179,184 , , 208. । । । । | , । । '| | । । T । । i1—r y r *i r । | i* | r i । "rmt-rfret“lI । । । । । । i1 n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #89099: Benzoic acid, p-anilino-, methyl ester 2.7 40.20 40.40 40.60 40.80 196 m/z 225.10 14.56%

5000 167 98 . 41 51 6577, 1 115 128 139 1| 180 /z—> 40 60 80 100 120 140 160 180 200 220 240 40.20 40.40 40.60 40.80

08428.D SCAN020418.M Thu May 02 15:36:09 2002 Page 7

NYC-WTC_000048205

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NYC-WTC_000048169

Laboratory report documenting GCMS analysis of sample AE08426 conducted on May 6, 2002, including surrogate recovery data.

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