GCMS scan report for Method 508, April 2002

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Data File : C:\MSDCHEM\1\DATA\020419\08485.D Vial: 22 Acq On : 20 Apr 2002 4:48 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 9 3-Azabicyclo[3.3.0]octane, . Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

40.44 0.57 ug/1 1019620 Chrysene-dl2 39.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Azabicyclo[3.3.0]octane, 7-iso... 227 C16H21N 1000156-34-6 40 2 5-Cyano-8-dimethylamino-6-methox... 227 C13H13N3O 1000213-20-5 36 3 4-Methyl-9-chloro-acridine 227 C14H10C1N 1000147-94-5 9 4 5-Cyano-2-methyl-6-phenyl-4-thio... 227 C12H9N3S 013996-07-1 9 Abundance Scan 6359 (40.442 min): 08485. D (-6341) (-) m/z 227.20 100.00% 2.7

5000 113 ■ ■ i ■ 40 85 99 198 I 40.20 40.40 40.60 40.80 ."090—0001—001111 , Mi ~ l, , , । III 240 oV m/z 113.50 27.05% n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #89074:3-Azabicyclo[3.3.0]octane, 7-isopropylidene-3-phenyl- 227

5000 91 144 158 .... L,.... 40.20 40.40 40.60 40.80 77 106 m/z 228.10 16.76%I 27 41 | 53 67 . 120130 , 170 184 193 212 0- 1)i 1. 141 I (1, ' r . pl, । 'll''.. '4. lt. | , ,1., ,1 ,r1 I,1 111 , ' I,j ,* •, .1 11 n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #89117:5-Cyano-8-dimethylamino-6-methoxyquinoline 227 212 M.................................................... 40.20 40.40 40.60 40.80 5000 m/z 226.20 15.11%|

198 42,52 63 76 88 101 114 127 141 155 169 184 | 0V ' ' ■ i 1 1 1 ■ !" ' । । । । ' । < । ■ । ■ ■ । । > । ■ EFL ■ > । । > ■■ > ■ । " । i-'i /z—> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #89143:4-Methyl-9-chloro-acridine 2.7 40.20 40.40 40.60 40.80 rn/z 225.10 9.72%

5000

191 63 82 96 114 139 163 01 i ' ' ■ ' i ' ' ■ ' i ‘ ■'l"1'"' 1 1 1 I ' 1 ' ( 1 ■ ■ i । 1, । । । । । ->-r-|-r-r t—>■ i > ■ । ■ r1 ■ ■ i ‘ ' 1 ■ i ■ ■ iz-> 20 40 60 80 100 120 140 160 180 200 220 240 40.20 40.40 40.60 40.80

08485.D SCAN020418.M Mon Apr 29 08:31:14 2002 Page 22

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