GCMS analysis results, Sample AE08262, April 22, 2002

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GCMS analysis report for sample AE08262 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048309–000048332

Folder label: “GCMS X 4/9/02 A 4/17/02”

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Data File : C:\MSDCHEM\l\DATA\020417\08262.D Vial: 19 Acq On : 18 Apr 2002 12:18 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 15 3-Azabicyclo[3.3.0]octane, . Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

31.46 0.28 ug/L 364689 Chrysene-dl2 30.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Azabicyclo[3.3.0]octane, 7-iso... 227 C16H21N 1000156-34-6 32 2 Silicic acid (H6-Si2-07), hexame... 258 C6H18O7S12 004371-91-9 23 3 Phenol, 2-(2-benzothiazolyl )- 227 C13H9NOS 003411-95-8 9 4 5-Cyano-2-methyl-6-phenyl-4-thio... 227 C12H9N3S 013996-07-1 9 Abundance Scan 4830 (31.458 min): 08262.D (-4819) (-) m/z 227.10 100.00% 217 149

40 5000 57 113 167 71 86 99 TT 198

ti/z—> 0- 20 40 60 80 | IM 100 120 140 160 180 200 220 I.... . I 240 — 240 31 20 31.40 31 60 31 80 m/ z 149.00 72.85% Abundance #89074' 3-Azabicyclo[3 3.0]octane, 7-isopropylidene-3-phenyl- 217 144 158

5000 "IT ‘I’" 91 31 20 31.40 31 60 31 80 77 106 212 m/ z 40.00 51.32% , 170 184 198 Qi 27 11 51, , 67 ' "h ' L -pual ., h । l ■ II, , J, , la, 1 , - I‘II‘‘‘I I 1 111 I 1 '■ i 120130

n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #89125: Silicic acid (H6-Si2-07), hexamethyl ester 2: 7

197 31.20 31.40 31.60 31.80 5000 m/z113.60 28.75% 167 91 107 121 137 151 181

Tl/Z—> Qi 45 61 77 । —IPmmmm । 1 ■ ' i ‘133 |' । ...... । 20 40 60 80 I, i J , ,|,i I ll 100 120 140 160 180 । । Ju 200 220 240 Abundance #127060: Phenol, 2-(2-benzothiazolyl)- 1 1 i ' 1 ' ' i ' ' ll l..... ' I ' ■ ■ ' I ' 1 227 31.20 31 40 31.60 31 80 . m/z; 57.00 27.84% 5000- 199

Tl/Z--> 0 20 39

40 60 69

15,27.4/544 "="-r4a4a—,—-t 1** , 1**1+ 1*i । i1, , ti । 80 36 | | 99 109 | 122 100 120 140 154 140 160 173 । 186 180 । 200 220 .1 240 A yA 31.20 31.40 ‘i’’ 31.60 31 80

08262.D 041702SCAN.M Thu Apr 18 09:49:34 2002 Page 20

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