GCMS sample AE12676 results, June 6 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\060402\12676.D Vial: 7 Acq On 4 Jun 2002 8:44 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C: \DATABASE\NIST98 . L

Peak Number 9 IH-Azonine, octahydro- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T.

5.02 0.33 ug/L 217472 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l lH-Azonine, octahydro- 127 C8H17N 005661-71-2 9 2 lH-Azonine, octahydro- 127 C8H17N 005661-71-29 3 Crotonic acid 86 C4H602 003724-65-0 7 4 Thiazole, 4-ethyl-2-methyl- 127 C6H9NS 032272-48-3 5 Abundance Scan 331 (5.024 min): 12676.D (-321) (-) m/z 128.90 100.00% 84 129

5000 47 40 4.60 4.80 5.00 5.20 5.40 Of ........................... ... ............................................... ■■i■1 ■ 1 f 1 1 1 i11 111'11 11■■'।।1111 11 '11 11 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ m/z 84.00 86.46% iz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #744: IH-Azonine, octahydro- 33 43 56

70 5000 127 4.60 4.80 5.00 5.20 5.40 84 m/z 126.80 74.35% 98 15 112

n/z-> ol 0 10 20 30 +37 +44944 60 70 80 90 100 110 120 130 40 50 91 TTTtT -

Abundance #108185:1H-Azonine, octahydro- 33 43 56 i ■ ■ ■ ■ i ' ■ ' 1 1

70 4.60 4.80 5.00 5.20 5.40 m/z 86.00 65.32%

"uLR 5000 127 84 96

iz-> Ot 15 +494 4 93.11., 78.1 .1,19 ■ ■ i1 111 ■'! ■ 1Ir , 37 10 20 30 40 50 60 70 80 3 112.179 , — 100 110 120 130 90 — 90 Abundance #116766: Crotonic acid 41 86 4.60 4.80 5.00 5.20 5.40 m/z 47.10 33.97% 5000 69

m/z-> 0 P 10 15 a 27 50,57. - —I,TTTT 1’l 20 30 40 50 60 70 80 90 100 110 120 130 । • ■ ■ ■ । ■ ■ ■ > । ' i ■ ■ ■ ■ i ■ ■ 4.60 4.80 5.00 5.20 5.40

12676.D 060302.M Wed Jun 05 14:04:42 2002 Page 12

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