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GCMS analysis results, Sample AE08262, April 22, 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08262 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048309–000048332

Folder label: “GCMS X 4/9/02 A 4/17/02

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Scanned page image, NYC-WTC_000048330
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020417\08262.D Vial: 19 Acq On 18 Apr 2002 12:18 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 trans-3-Phenyl-perhydrocycl... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

30.03 0.36 ug/L 472216 Chrysene-dl2 30.88

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 trans-3-Phenyl-perhydrocyclohexa... 244 C14H16N2O2 1000144-99-0 7 2 cis-3-Phenyl-perhydrocyclohexano... 244 C14H16N2O2 1000148-15-5 7 3 6-Chrysenol 244 C18H120 037515-51-8 5 4 1,4-Cyclohexadiene, 6-methylene-... 244 C19H16 018636-59-4 5 Abundance Scan 4588 (30 036 min): 08262.D (-4586) (-) m/z 244.05 100.00% 40 244

85 5000 54 109 122 212 — 73 11*’’I’ 96 29.80 30.00 30.20 30.40

/z-> O'I-------- -- 20 40 III I 60 ih. 120 11.80,m.. 100 140 160 180 200 220 240 m/z40.00 89.23% Abundance #92116: trans-3-Phenyl-perhydrocyclohexano[d]pyrimidin-214. . 93 24.4

119

5000 1T 29 80 30.00 30.20 30.40 81 41 54 67 148 m/z 243.10 60.19% 27 109

n/Z—> o ।'''' 1L 20 h I 40 60 80 100 4. I, 120 140 160 180 — 200 220 202 216

240 Abundance #92131 cis-3-Phenyl-perhydrocyclohexano[d]pyrimidin-2,4-dion 93 11 9 24.4

29 80 30.00 30.20 30 40 5000 m/ z 85.10 55.00% 41 54 67 81

271,1/1111109 I...... I........ 139 292 216 ... 0 I ........... I* ' 11 I ....... f I ' 1 1 r l......... 148 J n/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #92175: 6-Chrysenol 2 5 24 4 ■ ■ i 1 1 ' 1 i ' —4 29.80 30 00 30.20 30.40 m/ Z 54.10 38.65%

5000 108

95 122 189 .... 41 51 63 81.11, —1|—— 163 , 0 | ' I ' I | '■ 7 । | । llr | ' f 1 1 | ''IT 139150 176 200 ....... 11 1 1 1 1 1 ' ’I1 T’T 1 1 I f ' n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 29.80 30 00 30 20 30.40

08262.D 041702SCAN.M Thu Apr 18 09:49:33 2002 Page 19

NYC-WTC_000048330

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NYC-WTC_000048330Source: NYC Law Department, mirrored locally

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