GCMS analysis results, Sample AE08262, April 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08262.D Vial : 19 Acq On : 18 Apr 2002 12:18 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Tetradecanamide Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

29.99 0.72 ug/L 948357 Chrysene-dl2 30.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetradecanamide 227 C14H29NO 000638-58-4 86 2 Tetradecanamide 227 C14H29NO 000638-58-4 78 3 Hexadecanamide 255 C16H33NO 000629-54-9 78 4 Heptanamide, 4-ethyl-5-methyl - 171 C10H21NO 054789-40-1 72 Abundance Scan 4581 (29.995 min) 08262.D (-4573) (-) m/z 59.05 100.00% 59

5000 72

— ———————— 86 97 114 128 142 240 29.60 29 80 30.00 30 20 30.40 184 207 0— m/z 72.00 44.86% Tl/Z-> 20 80 100 120 140 160 180 200 220 240 260 Abundance #113299 Tetradecanamide 59

5000 ■ ■ i ■ ■ ■ i ■ ■ 72 29 60 29.80 30.00 30.20 30.40

/z-> Abundance

5000 0- -H 20 40 28

41 43

1 i [ V । । Arroa | 1 !i । । 60

59

72 80 86 98 100 114 1 28 120 1 49 140 #19652: Tetradecanamide 170 1 84 198 | liii [I , * , । , । । । । । । । < । i ~ | i 160 180 200 220 240 260 227 m/z

PMA 43.10

29 60 29.80 30.00 30.20 30.40 m/ Z .K 57.10 23.60%

17.09%

29 1

n/z-> 0^ -1841 8086 98100 114120128 140142 156160170180184 198200210220. ... 20 40 60 240 260 Abundance 59 #113298: Hexadecanamide A/ 29 60 29 80 30 00 30.20 30.40 m/z 55.10 16.10% 5000 72

43 0 29 1 1 1 I 1 1 1 1 17 86 97 , । r, > 114 1 28 142 155 170 184 198 212 226238 255 T* .■■. । । । I । । । । r, . । । । . I । । । . ■I ' —4 444, . 1 /Z- > 20 40 60 80 100 120 140 160 180 200 220 240 260 29.60 29 80 30 00 30 20 30.40

08262.D 041702SCAN.M Thu Apr 18 09:49:33 2002 Page 18

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