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GCMS blank results for volatile organics, April 2002

Machine-extracted title · confidence 100%

Laboratory report showing blank analysis results for volatile organic compounds in sample AE08260 from April 2002.

NYC-WTC_000048225–000048255

Folder label: “GCMS X 4/9/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\0409LB.D Vial: 4 Acq On : 17 Apr 2002 11:51 am Operator: Nefliu Sample : 04/09 1b Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C: \MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Heptadecane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

21.82 1.00 ug/L 1116490 Phenanthranene-dl0 23.02

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 96 2 Heptadecane 240 C17H36 000629-78-7 93 3 Heptadecane 240 C17H36 000629-78-7 93 4 Heptadecane 240 C17H36 000629-78-7 91 abundance Scan 3190 (21 822 min): 0409LB D (-3180) (-) m/z 57.10 100.00% 57 43 71 5000 85 ----- 00 1 35 -P

n/z- > 0- 120r 1 1 14014— 60 + —r .. Il . 1 4, 125 .I r ■ ■ 80 i 113, I 100 120 140 154 169 182 160 180 200 220 240 240 21.40 :21.60 21 80 22.00 22 20 m/z 43.10 65.22% abundance #16420 Heptadecane 57 43 71 85 5000- 21.40 21.60 21 80 22.00 22 20 29 99 m/z 71.10 59.07% 1 113 127 141 155 169 183 197 211 240 0- 115.1, ' 1 i 1 ‘ 1 1 i 1 1 ' ' I ■ ' 200 220 240 Tl/Z—> 20 40 60 80 100 120 140 160 180 Abundance #112322' Heptadecane 43 57 --P 21 40 21 60 21 80 22.00 22.20 71 5000 m/ z 85.10 43.60% 85 29 99 113 127 141 155 169 183 197 211 240 0- - rr " । ’1 । "hi . 1 . , I1. । 14l IA*/vr r. । i-i |r n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #112319: Heptadecane 1"* । f i*i *" । 17*7 rl i*| . , 7 21.40 21 60 21.80 22.00 22 20 43 m/z41.10 31.23% 71 5000 85 29

Tl/Z-> 0 "'I 14 ' ' 'I11' 20 40 U 60 99 113 127 141 155 169 183 TT9——0—m/mmm——m)OTTTTT 80 100 120 140 160 180 200 220 240 240 XAMMMPCAPY 21.40 21.60 21 80 22.00 22.20

0409LB.D 041702SCAN.M Thu Apr 18 09:42:00 2002 Page 12

NYC-WTC_000048239

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NYC-WTC_000048239Source: NYC Law Department, mirrored locally

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