GCMS analysis results, Sample AE08265, April 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08265.D Vial: 22 Acq On : 18 Apr 2002 2:44 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Muitiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 9 Heptadecane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

21.82 0.27 ug/L 455760 Phenanthranene - dl 0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Quad

1 Heptadecane 240 C17H36 000629-78-7 95 2 Heptadecane 240 C17H36 000629-78-7 93 3 Heptadecane 240 C17H36 000629-78-7 90 4 Pentadecane___________________________ 212 C15H32 000629-62-9 87 Abundance Scan 3190 (21.822 min): 08265.D (-3181) (-) m/ z 57.10 100.00% 57

43 71 5000 85

1 , 14 n r rA , T l ,* I p ,~l 99 12 4.4.4.18,127....24° 21.40 21.60 21 80 22.00 22.20 0 TI——m— m/z 71.10 62.85% n/z- > 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #16420. Heptadecane 57 43 71

5000 85 . .... MM 21.40 21.60 21.80 22.00 22.20 11**

29 99 m/z 43.10 59.56% 1 113 0- 154 , l J 141 ,155,160169.183 n ..1.4 140 197,211 240 n/z-> 20 40 60 80 100 120 180 200 220 240 Abundance #112319 Heptadecane 43 57 71 21.40 21 60 21 80 22.00 22.20 5000- m/z 85.10 46.59% 85 29

n/z-> 0- ■ i 14 20 40 U h । 1-^ 99 113 127 141 155 169 183 60 80 100 120 140 160 180 200 220 240 240 Abundance #112320 Heptadecane _ 4* "ki..... 57 21 40 21.60 21.80 22 00 22 20 43 m/ z 41.05 34.14% 71 5000 85 29 — 99 J 113 127 141 155 leg 182 196 210 0 +— "I si 4 .if.. Ii . i' । । ■ i । । r. , । , 240 wwptuanhnnnd/ “Yut bajw n n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 21 40 21.60 21 80 22.00 22 20

08265.D 041702SCAN.M Thu Apr 18 09:58:19 2002 Page 14

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