GCMS analysis results for sample AE10610, May 10 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\l\DATA\050702\10610.D Vial: 13 Acq On 7 May 2002 10:55 pm Operator: Mclean Sample 5/3 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Hexadecanamide Concentration Rank 4 R. T. EstConc Area Relative to ISTD R.T. 29.92 0.34 ug/L 367709 Chrysene-dl2 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecanamide 255 C16H33NO 000629-54-9 78 2 Dodecanamide 199 C12H25NO 001120-16-7 59 3 Tetradecanamide 227 C14H29NO 000638-58-4/59 4 Tetradecanamide 227 C14H29NO 000638-58/4 50 Abundance Scan 4568 (29.919 min): 10610.D (-4560) (-) m/ z 59.10 100.00% 59

5000 72 ................................................... 43 29.60 29.80 30.00 30.20 ......... I , ,l,l , 86 98 114 128 ■ [ ' ‘ 240 l 1 > 1 ■' I 1 ' 1 ' J ' 1 ' ' I 1 ‘ 1 1 I 1 ■ 1 1 I ' ' > 1 I I '■ ■■ 1 I I I I ■ I I m/ Z 72.10 46.26% /z->20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #113298: Hexadecanamide 59

5000 72 ---P— ______ 1 I ‘ ________ ' I ' ' 1 1 1 1 1 1 ' I 29.60 29.80 30.00 30.20 m/z 43.10 26.09% 86 100 114 128 t42 -i56 170 184 198 212 226238 255 ■ ' 1 i ■ Tr 11 i " । 1 | i Hi r - 1 ■ *| । rh i—j I—। । i—।—i—r I i ]—i1 r i ——i—P—r m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #19649: Dodecanamide 59 % Al-A4—— ‘ ‘ I ' ' 1 ' 1 1 1 1 1 I 29.60 29.80 30.00 30.20 5000 m/ Z 41.20 19.18%

U 72 28 43

15 i ||| , 86 100 114 128 142 156 170 199 ■ 1 ' i ’ 1 | ' 1T" 1 1 । 1 । ' । 1 > |' । । 1" । 1 i । । ■ । । 1 I' । । ।1 > । । i । । ' 1 । ■ । । । । । । । । । ।—। ।11 m/z->______ 20 Abundance 40

59 60 80 100 120 140 #113299: Tetradecanamide 160 180 200 220 240 260 —Antep 29.60 29.80 30.00 30.20 m/ Z 55.10 15.44% 5000 72 f

43

m/z-> 28 . th .. |l . , .. 86 98 .■ 114 128 149 170 184 198 m [ , 'I1"! I। । I । । | 20 40 60 । r r । । 11 I I | r । i । । I iii । ’ > i i I | i I' i 1 । | in “i11 ■ r'

80 100 120 140 160 180 200 227 ' ' i 1 '' ' ' 1 1 1 1 ' i 1 220 240 260 1B.1 29.60 29.80 30.00 30.20 A ' I 1 ’ ' 1 1

■ 10610.D 050102.M Thu May 09 09:15:27 2002 Page 10

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