GCMS analysis results for sample AE10610, May 10 2002

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Laboratory report detailing GC/MS analysis of sample AE10610 including surrogate recovery data in May 2002.

NYC-WTC_000045662–000045681

Folder label: “GCMS X 5/3/02 A 5/7/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\l\DATA\050702\10610.D Vial: 13 Acq On 7 May 2002 10:55 pm Operator: Mclean Sample 5/3 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Trifluoroacetic acid, n-hep... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 30.17 0.24 ug/L 257149 Chrysene-dl2 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trifluoroacetic acid, n-heptadec... 324 C17H31F3O2 1000216-79-2 5 2 Trifluoroacetic acid, n-tetradec... 310 C16H29F3O2 1000216-79-0 / 9 3 1-Nonadecanol 284 C19H40O 001454-84-8 7 4 1-Eicosanol 298 C2OH420 000629-96- / 43 Abundance Scan 4611 (30.172 min): 10610.D (-4602) (-) m/ z 43.10 10 . 00% 43

5000 57

70 83 97

111 125 L M— “YunAAdu—l I | r i | i | TLUi1/1/1/1/d/gn

I I 1 ' ' 1 1 ] -rn~]-T-r-r-r-p-r T rq । U i i । I I i । i । । । । । i । । । । r 29.80 30.00 30.20 30.40 30.60 m/Z 57.10 71.47%' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #4324: Trifluoroacetic acid, n-heptadecyl ester 43 57

5000 70 83 97 L 29.80 30.00 30 20 30.40 30.60 m/ Z 69.10 63.96%

m/z-> 1 1 1 1 20 40 JU 60 80 d 111 | T | 14 140153 I IT i 182 210 | I i i f | i 1 I i । i i i i । ' i IT 7 । T" T i ' i ।

100 120 140 160 180 200 220 240 260 280 sv i । i i i I | iiii । i i

Abundance #4218: Trifluoroacetic acid, n-tetradecyl ester 43 I I I I I I I I I I I "Inn I I I — I I 57 29.80 30.00 30.20 30.40 30.60 5000 m/z 97.10 H 63.86% 83 70 97 111 I 125 140 155168 196 11 I ' 1 I I r I I r I I I [ I F I I I I I I I I t I u - r | iii'i । iTi — n 1 | iiii 1 r m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #4327:1-Nonadecanol Tgr 1 1 i 1 1 ' ■ i 1 43 29.80 30.00 30.20 30.40 30.60 57 m/ z 55.10 62.54% 29 5000 83 /0 97

/z-> 154 20 40 -1ul—44r || t J, 125 140154 168182 196 210 224 238 252 266 280 60 80 it i ff 1 | 1* 1 1 "| 1 1 1 | 11 ' ' | 1 1 1 1 I 1 1 1 । | । 1' । "I 100 120 140 160 180 200 220 240 260 280 I" IT ! [ 1" I I IPrI ' i 1 r 29.80 30.00 30.20 30.40 30.60 1 ' 1 1

10610.D 050102.M Thu May 09 09:15:30 2002 Page 11

NYC-WTC_000045677

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