GCMS sample analysis results for AE10606, May 10 2002

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Laboratory report detailing GC/MS analysis of sample AE10606 including surrogate recovery data in May 2002.

NYC-WTC_000045624–000045642

Folder label: “GCMS X 5/3/02 A 5/7/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050702\10606.D Vial : 11 Acq On 7 May 2002 9:17 pm Operator: Mclean Sample 5/3 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 Phosphonic acid, dioctadecy... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.00 1.07 ug/L 1051930 Chrysene-dl2 30.81

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9 64 2 Trifluoroacetic acid, n-heptadec... 324 C17H31F3O2 1000216-79-2 6 3 11-Tricosene 322 C23H46 052078-56-5 62 4 1-Octadecene 252 C18H36 000112-88-9/58 Abundance Scan 4412 (29.002 min): 10606.D (-4405) (-) m/z 55.10 100400% 55

83 5000 111 / TT TT :l 127 28.60 28.80 29.00 29.20 29.40

m/z-> —144 80 100 dk1204 140H 160 180 200 220 240 260 280 300 320 20 40 60 i11 r 11 ■ ■ ■' ।11 ■1111 m/z 57.10 54.64% Abundance #13890: Phosphonic acid, dioctadecyl ester 55 83

A___ j "Wooniow) 5000 । i i । । । i i + । । । i i i । । I । I । f <

111 28.60 28.80 29.00 29.20 29.40 29 136 m/ z 43.20 53.30% 14 I HH r 151 'i ■ ■ ■ 1 i 111’’111111111101*310113*1111111"1Ih1T m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #4324: Trifluoroacetic acid, n-heptadecyl ester 43 1A M MM AMMpysw,A/ 69 28.60 28.80 29.00 29.20 29.40 5000 m/ Z 83.10 A 50.57% 97 4. 112 k 140155 182 210 v 19d—aum*uumunupT] m/z--> Abundance 20 40 V 60 80 100 120 140 160 180 200 220 240 260 280 300 320 #4287: 11-Tricosene I ' 1 1 1 I I ' 1 1 ‘ i 1 ' ' 1 I '

_____________ _AAAAA I I I I I ill I > 1 I I I I "I ( "1 11 73 I v 43 28.60 28.80 29.00 29.20 29.40 m/z 73.10 46.37% 83 5000

111 8 Il 126 . 154 183 210 238 266 294 322 1 1 i ' ■ ' ■ i' ■ TT ’ ITi i " i । T i i i | i i F r । I I i i pi i i I । ■ i I I | I I I I | I | I I | ■ i I I । I I I | | | | | ) | *| T /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 28.60 28.80 29.00 29.20 29.40

10606.D 050102.M Thu May 09 09:12:11 2002 Page 12

NYC-WTC_000045640

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