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GCMS sample analysis results for AE10606, May 10 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GC/MS analysis of sample AE10606 including surrogate recovery data in May 2002.

NYC-WTC_000045624–000045642

Folder label: “GCMS X 5/3/02 A 5/7/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050702\10606.D Vial: 11 Acq On 7 May 2002 9:17 pm Operator: Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.54 ug/L 628883 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO - 188 C14D10 001719-06-8 94 2 Phenanthrene-dlO 188 C14D10 001517-22-2 80 3 7-Tetradecene-5,9-diyne, (E)- 188 C14H20 013304-98-8 42 4 2-Quinolinecarboxaldehyde , 8-hyd... 188 C10H8N202 005603-22-5 40 Abundance Scan 3409 (23.109 min): 10606.D (-3403) (-) m/z 188.10 100.00%| 188

5000

..0’)..) " mpr i 43 57 80 94 22.80 23.00 23.20 23.40 S-1 1 [ I 1 ■ I 1 1 14p | 1, 132 160 |, 253 268 m/z 189.10 16.13% 1 c H 1 1 1 1 1 1 1 1 1 ' 1 I 1 1 1 '1 1 1 1 ' I'1 ■ । | 1 1 ' ■ | ■ 1 1 1 | ■ ■ !’ । | । 1 1

m/z->______ 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #79826: Anthracene-d10- 188

5000 ) 22.80 23.00 23.20 23.40 m/Z 80.00 13.55% 80 94 160 I, 28 40 52 66 I ,I I I'll J |106118 132 146 I I 1 1 1 1 1 1 1 1 I1 —Hr —4 I I I I | ' I ! I I | 1 I " I | I I | "I' ‘ । , । , | | | | | | | | | Cl | ' | |' | J

/z->______ 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/ z 184.05 12.91%

80 94 160 28 40 52 66 IlIl I 108120132 146 +4, , ! , 41, , | ! I । । । । । । । । i'i । i'i , l1) , > I I I I I ill I I ’ I I 1 1 i ■ ■ ■ 1 i 1 ' 1 1 i ■ ■

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #79740: 7-Tetradecene-5,9-diyne, (E)- ■ ■ । ■ ■1 1 i 1 1 188 22.80 23.00 23.20 23.40 117 131 m/z 57.10 11.77% 91 5000 41 77 103 145

Tl/Z-> ................. I........ 1 1 i ' 1 1 1 i ' ' 1 ■ i ■ 1 20 40 60 80 100 1, 11 , 159 1 ' i ■ ■ 1

120 140 160 180 200 220 240 260 1 i 1 22.80 23.00 23.20 23.40 1 ' i 1 1

10606.D 050102.M Thu May 09 09:12:09 2002 Page 11

NYC-WTC_000045639

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NYC-WTC_000045639Source: NYC Law Department, mirrored locally

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