NYC-WTC_000045643
Laboratory report detailing GC/MS analysis of sample AE10609 including surrogate recovery data in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 19 pages
GCMS sample analysis results for AE10606, May 10 2002
Machine-extracted title · confidence 100%Laboratory report detailing GC/MS analysis of sample AE10606 including surrogate recovery data in May 2002.
NYC-WTC_000045624–000045642Folder label: “GCMS X 5/3/02 A 5/7/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050702\10606.D Vial : 11 Acq On 7 May 2002 9:17 pm Operator: Mclean Sample 5/3 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L ********************************************************************* Peak Number 10 Vanadium, toluene-cyclopent... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 30.97 0.29 ug/L 283084 Chrysene-dl2 30.81
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Vanadium, toluene-cyclopentadienyl- 208 C12H13V 1000153-69-1 5 2 1,1'-Biphenyl, 2-methyl-4,5-meth... 212 C14H1202 093044-85-0 5/ 3 4,5-Dichloro-N-methyl -1,3[3H]-ox... 195 C5H3C12NO3 1000214-40-84 4 2,4'-Dihydroxy-stilbene 212 C14H1202 1000147-73-5 3 Abundance Scan 4747 (30.971 min): 10606.D (-4746) (-) m/z 43.20 100.00% 43 116
5000 212 234 h Jw 55 104 1 1 i 1 1 ' 1 1 1 ' i 1 1 CpT
m/z-> 20 — 40 II , , 92 1 1 1 1 1 1 1 ' i ■ ' ' 1 1 1 1 i 1 ’ ' 1 i 1 1 ‘ 1 I ' 1 1 1 I 1 1 ' 1 I 1 30.60 30.80 31.00 31.20 31.40 m/z 116.20 67.58% 60 80 100 120 140 160 180 200 220 240 Abundance #52199: Vanadium, toluene-cyclopentadienyl- 1- 6
5000 ' i 1 1 TT 30.60 30.80 31.00 31.20 31.40 208 51 m/z 234.00 56.06% 90 27 39 I 65 76 1 i 1 1 1 ' T ‘ 1′11 ■' 1 ।1 +104 । 128 140 153 166 179 194 । । i r de r i l ll I l [ i '1 i । i ' ' i 1 1 ' ' i ' m/z-> 20 40 60 801 100 120 140 160 180 200 220 240 Abundance #85926:1,1’-Biphenyl, 2-methyl-4,5-methylenedioxy- 2 2
30.60 30.80 31.00 31.20 31.40 5000 m/z 212.00 54.85% 118 76 91 104 152 181 41 51 63 । 4 90139
iT । । । ll apullpda ■lrl|l"l'"A. ..li 1,411124,144,1654,, 1 200 '' I ' ' — 11
m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #52126: 4,5-Dichloro-N-methyl-1,3[3H]-oxazine-2,6-dione 1 6 30.60 30.80 31.00 31.20 31.40 m/z 111.10 54.55%
5000 88 52 151 63 76 195 .....41 |1 +lUMLC i 1 1 1 ' i 1 1 126 I 140 1 [ I > |.161 179 I, I I I I I I I I I I I I I ■ I 1 I I > I I I I I I I I I 1 .......... IIII I /A I I k I A_______ A 1 ' i 1 1 1 1 i 1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 30.60 30.80 31.00 31.20 31.40
10606.D 050102.M Thu May 09 09:12:14 2002 Page 13
NYC-WTC_000045641
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