GCMS sample analysis results, AE11906, June 3, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11906.D Vial: 13 Acq On : 22 May 2002 11:36 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Toluene Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 4.28 2.04 ug/L 1582300 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# ual

1 Toluene 92 C7H8 000108-88 74 2 Toluene 92 C7H8 000108-88-3 72 3 Toluene 92 C7H8 000108-88-3 72 4 Cyclobutene, 2-propenylidene- 92 C7H8 052097-85-5 64 Abundance Scan 205 (4.284 min): 11906.D (-195) (-) m/ z 91.10 100.00% 91

5000

35 39 65 4.00 4.20 4.40 4.60

miz—> 4-HTTHPH IWTTTTTTTTTT O' TTIWOIWTTTTTTTTH 87 - 46 50 15 20253035404550556065 70 75 80859095 100 58 m/z 92.10 59.85% Abundance #37326: Toluene 91

5000 *’**I*’*I+111*** 4.00 4.20 4.40 4.60 m/z 35.10 17.14%

miz-> Abundance 27 31 39 45 51 57 61 65 73 77 86,, 0- 1 ‘ l ■ “ ' I ■ m |'1.. I ■. I,! H I l't' 11111.. i [ 1' ■ ■ p.1 .'11! 11) 11.. i. , I. I.!.. I ■. r.!.!. 11 — 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 #117283: Toluene "MMwi, "Mrh 91

4.00 4.20 4.40 4.60 5000 m/z 65.10 13.53% 39 65 27 45 51 35 23 j 31 — 0 TIIWTLTTHTT .35411417444,56...61 73 77 81 86 ,, 1Dmmm HP miz-> Abundance 15 20253035404550556065 70 7580859095 100 #117282: Toluene 91 4.00 ll,.. — 4.20 4.40 4.60 m/z 39.10 10.46%

aals 5000

39 E 65

/z—> 0 ................ ,1,,.^..°,.... ................ 86.1 । 'i '"‘i" 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 4.00 4.20 A 4.40 4.60

11906.D 052202.M Tue May 28 12:13:16 2002 Page 10

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