GCMS sample analysis results, AE11902, June 3, 2002

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Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11902.D Vial: 9 Acq On : 22 May 2002 8:20 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ************** *k ***************************************************** Peak Number 10 Toluene Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

4.27 2.05 ug/L 1319980 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Q 1 Toluene 92 C7H8 000108-88-3 80 2 Toluene 92 C7H8 000108-88-3 80 3 Toluene 92 C7H8 000108-88-3 80 4 Toluene 92 C7H8 000108-88-3 72 Abundance Scan 203 (4.272 min): 11902.D (-198) (-) m/z 91.10 100.00% 91

5000 Um

n/z-> 0- ........... 0 10 2030405060 3s„5Q..58,T7.,.. ,.85 70 8090 I, , 100 m/z 4.00 4.20 92.10 4.40 4.60 71.17% Abundance #117282: Toluene 91

5000 4.00 4.20 4.40 4.60 m/z 65.00 12.17% 0- 27 T 45 51 * demhna cIttily chea r i (’ll i f i !•:•> | I nt i f5 77 86,, n/z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #117292: Toluene 91

4.00 4.20 4.40 4.60 5000 m/z 39.10 10.72%

39 51 65 27 J 45 ? 57 I.I 77 86,J 0- —I=9TR—0100+1—-—-.m1) j_________ • 1 1 1 ’ nz-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #117281: Toluene 91 4.00 4.20 4.40 4.60 m/z 43.10 9.11% 5000

39 45 51 65 27 n/z-> 0- 1 1 ' T‘ • • 1 1 1 0 10 15 ' 1 1 111, — 20 30 +446+456 40 50 + 41— 60 70 7780—86490 1100 1 1 i ■ ■ ■ ' i ■ ■ ■ ■ i ■ 1 ■ ■ i ■ ■ 4.00 4.20 4.40 4.60

11902.D 052202.M Tue May 28 12:06:39 2002 Page 13

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