NYC-WTC_000023904
Laboratory report showing GC/MS analysis of sample AE10981 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Document / 31 pages
GCMS analysis results, sample AE09154, May 2002
Machine-extracted title · confidence 100%GCMS analytical report for environmental sample AE09154 including surrogate compound data from May 15, 2002.
NYC-WTC_000022819–000022849Folder label: “GCMS X 5/8/02 A 5/10/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\050902\9154.D Vial: 19 Acq On : 10 May 2002 6:47 am Operator: Mclean Sample : 5/8 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 (IS,2S)-1,2-Dihydroxy-3,14-.. Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
34.94 0.42 ug/L 249952 Perylene-dl2 34.70
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 (IS,2S)-1,2-Dihydroxy-3,14-dioxo... 262 C10H18N2O6 1000111-03-0 1 2 Vanadium, (. eta. 7-cycloheptatrie . . . 207 C12H12V 012636-68-9 12 3 Vanadium, (.eta.7-cycloheptatrie... 207 C12H12V 012636-68-9 2 4 2-(1-Piperidino) -5-nitropyridine 207 C10H13N3O2 026820-61-1 5 Abundance Scan 5422 (34.936 min): 9154.D (-5421) (-) m/z 207.00 100.00% 207
84 191 5000 .129 116 256
96 34.60 34.80 35.00 35.20 -
I 0! i 1 1 ■ 1 i ' ■ ' 1 i ' ' ■ ' I m/z 83.90 51.77% n/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #23995: (1S,2S)-1,2-Dihydroxy-3,14-dioxo-7,10-dioxa-4,13-d... 70
5000 T" Tk" 34.60 34.80 35.00 35.20 58 85 101 129 262 m/z 190.90 47.12% 114 146 159 177 192204 218 245 | Of . all,+ 1 4 l, l, . 4—r । it11 ("rh i । !'■ । 4" । r"i । Mr । । i-i Ti IIIi m/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #84765: Vanadium, (.eta.7-cycloheptatrienylium)(.eta.5-2,4... 207
129 51 m/z 129.30 42.04% 5000 116
76 90
miz-> 27 39 0 1*‘7u‘ PI— 20 40 60 64 14 1 192- , 142 155 169 181193 i ■ ■111'1i1 ■' 1* 1 IT 80 100 120 140 160 180 200 220 240 260 Abundance #126462: Vanadium, (.eta.7-cycloheptatrienylium)(.eta.5-2,... IMAAAA I 7,1 1 I ' ‘ 1 1 I 207 34.60 34.80 35.00 35.20 m/z 127.90 38.27% 129 51 5000 116
n/z-> 0 Iauuuuv 20 39 40 76 90 -l 60 .. 142 1....... . 80 100 120 140 160 180 200 220 240 260 pmn.... 34.60 34.80 35.00 35.20
9154 .D 050102 .M Mon May 13 11:28:57 2002 Page 15
NYC-WTC_000022838
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NYC-WTC_000022838Source: NYC Law Department, mirrored locally
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