NYC-WTC_000024014
Laboratory report showing GC/MS analysis of sample AE10985 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Document / 32 pages
GCMS analysis results for sample AE09571, May 2002
Machine-extracted title · confidence 100%Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09571 conducted on May 14, 2002.
NYC-WTC_000023023–000023054Folder label: “GCMS X 5/8/02 A 5/9/02”
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OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\1\DATA\050902\9570.D Vial: 7 Acq On 9 May 2002 8:10 pm Operator: Mclean Sample 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Bicyclo[3.1.1]hept-3-en-2-o.. Concentration Rank 13
R.T. EstConc Area Relative to ISTD R.T.
28.12 1.54 ug/L 2678240 Chrysene-dl2 30.81
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Bicyclo[3.1.1]hept-3-en-2-ol, 4,... 152 C1OH160 000473-67-6 14 2 2-Propenamide, 3-(3,4-dihydro-2H... 138 C7H10N2O 035663-85-5 12 3 2-Oxaadamantane 138 C9H140 000281-24-3 11 4 Cyclohexanol, 5-methyl-2-(1-meth... 156 C10H20O 000491-0120 10 Abundance Scan 4262 (28.121 min): 9570.D (-4254) (-) m/z 71.10 100.00% 57 71
5000 40 82 95 109
119 138 EE 147155 167 179 191 ANN 127 27.80 28.00 28.20 28.40
m/z-> XI J 01 ■ i" " ।" " । till... — i' ■ " i ■' " i'1" i1''11 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 57.10 85.81% Abundance 41 #49149: Bicyclo[3.1.1]hept-3-en-2-ol, 4,6,6-trimethyl-
81 94 109 AMNuA 5000 55 69 27 27.80 28.00 28.20 28.40 119 m/z 109.00 77.16% 134
n/z-> OlTittf — 44lll+ +,1143’52., 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 11'1111"11 ■ " ' I pWhyrWWr"MMW Abundance #40854: 2-Propenamide, 3-(3,4-dihydro-2H-pyrrol-5-yl)-, (E)- 94 138 110 27.80 28.00 28.20 28.40 m/z 95.10 57.65% 5000 41 55 65 82 121 mMawMMytwAnyay n/z-> 0 TTT 28 T + 'I... K 11 " ‘ i'" 11 ■ ■ " r ' " i' " ' i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #40851:2-Oxaadamantane 94 138 27.80 28.00 28.20 28.40 m/z 111.10 57.65% 5000 41 55 70 81 AaM/wrnwnn 27 109 123
4HHHL 'l" i ■ ■ ■ ■ i ■ “■ i “ " i " " i “ " i
o ‘IT ir,. . lii', —ll n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 27.80 28.00 28.20 28.40
9570.D 050102.M Mon May 13 11:46:46 2002 Page 11
NYC-WTC_000023038
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NYC-WTC_000023038Source: NYC Law Department, mirrored locally
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