GCMS analysis results sample AE11926, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052302\11926.D Vial: 6 Acq On : 23 May 2002 2:02 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 Bicyclo(3.2.0]hepta-2,6-diene Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

4.27 0.66 ug/L 468138 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Bicyclo(3.2.0]hepta-2,6-diene 92 C7H8 002422-86-8 22 2 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2/16 3 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 9 4 1,3 ,.5-Cycloheptatriene 92 C7H8 000544-25-2 9 Abundance Scan 203 (4.272 min): 11926.D (-200) (-) m/z 91.10 100.00% 91

5000 38 51 58 65 86 100 ‘ M ' !4 4 ‘ 4 I ‘ ‘ ‘ ’ l —————— 4.00 4.20 4.40 4.60 --- m/z 92.10 49.41% O+ TIi 11 miz-> 10 20 30 40 50 60 70 80 90 100 Abundance #37273: Bicyclo[3.2.0]hepta-2,6-diene 91

5000 ...... 14...... 4.00 4.20 4.40 4.60 39 66 m/z 86.00 30.70% 0- ......... 27 ............... JI.......... । ■ ■ i • ■ • ■ i ■ ■ ■ ■ i • • ■ ■ I ■ ■ ■ ■ I' ' ■ ■ i ■ ■ 1 ■ i ■ ■ ■ • i 1 ■ ■ ■ i 1 ■ 1 i ■ ■ ■ ■ i niz-> 10 20 30 40 50 60 70 80 90 100 Abundance #117298:1,3.5-Cycloheptatriene 91

4.00 4.20 4.40 4.60 5000 m/z 38.00 23.10%

28 39 65 ft 01 ----- _ .11,45.51,60,1,1, 77 86 , 1 • ■ i • ■ ■ ■ I iz-> 10 20 30 40 50 60 70 80 90 100 Abundance #117284:1,3.5-Cycloheptatriene 1217 rvt 91 4.00 4.20 4.40 4.60 m/z 39.10 20.21%

5000 39 65

n/z—> 0 11151107722.1 10 20 30 40 45.41—469,1 50 60 | 72 77 + i i ' 1 ' ■ r ■ 1 •' ' l 70 80 86 , 90 ■ ' i ' ' ' 1 I 100 • I ‘ ' ‘ ‘ I ‘ ** ‘ I 4.00 4.20 4.40 4.60

11926.D 052202.M Wed May 29 09:47:51 2002 Page 12

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