GCMS sample analysis results, AE11903, June 3, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11903.D Vial: 10 Acq On : 22 May 2002 9:09 pm Operator: Mclean Sample : 5/21 ad Inst •: Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan "* Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 Spiro[2.4]hepta-4,6-diene Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 4.28 1.16 ug/L 853908 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# quay 1 Spiro[2.4]hepta-4,6-diene 92 C7H8 000765-46-8 53 2 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2/52 3 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 52 4 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 52 Abundance Scan 204 (4.278 min): 11903.D (-200) (-) m/z 91.10 100.00% 91

5000

* 39 49 65 84 4.00 4.20 4.40 4.60

miz-> 0- i ■' ■ ■ i ■1 ■ ■ i ' ■ ■ • i 1 010 20 30 458490 100 110 40 50 60 70 80 i m/z 92.10 49.44% Abundance #37322: Spiro[2.4]hepta-4,6-diene 91

5000 " I ■'" I 4.00 4.20 4.40 4.60 65 m/z 65.10 16.72% 27 39 45 51 59,(1, 77 85, 0- — ———————— —————————————————0—9——————— T-T-p-r-n-p-r m/z-> 0 10 2030405060 70 8090 100 110

.... a.... Abundance #117284:1,3,5-Cycloheptatriene 91

4.00 4.20 4.40 4.60 5000 m/z 39.20 13.04% 39 65 E 27 77 85 , 45 51 l 0 p miz-> Abundance 0 10 20 30 40 50 60 70 80 90 #37276: 1,3,5-Cycloheptatriene 91 100 110 _MAL 4.00 4.20 4.40 4.60 m/z 49.10 11.12% 5000- 39 65 15 27 .1 ,. 45 51 57 71 77 85 , 2 106 0- 1 ‘ i 1 • • 1 i 1 r‘ ‘ i ■ — i rI11*PiU i‘|Hi t । । 1’ti {• riTij1! miz-> 0 10 20 30 40 50 60 70 80 90 100 110 4.00 4.20 4.40 4.60

11903.D 052202.M Tue May 28 12:07:46 2002 Page 12

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