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GCMS analysis results for sample AE09571, May 2002

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Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09571 conducted on May 14, 2002.

NYC-WTC_000023023–000023054

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000023037
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050902\9570.D Vial: 7 Acq On 9 May 2002 8:10 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 Octadecane, 6-methyl- Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T.

27.69 1.50 ug/L 2614460 Chrysene-dl2 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane, 6-methyl- 268 C19H40 010544-96-4 38, 2 Undecane, 3-methyl- 170 C12H26 001002-43-3 35 3 Octadecane 254 C18H38 000593-45-3 27 4 Heptadecane 240 C17H36 000629-78-7 27 Abundance Scan 4189 (27.692 min): 9570. D (-4178) (-) m/z 57.15 100.00% 57

5000 43 71 85 wwAM4 98 121 138 153

0- m 11d —4 'Hi 11a 1u. 116 — 183 27.40 27.60 27.80 28.00 m/z 43.15 46.59% miz-> Abundance 20 40 60

57 80 100 120 140 160 180 200 #16226: Octadecane, 6-methyl- 220 240 260 WAMNy 43 28 5000 27.40 27'60 27'80 28.00 71 rn/z 71.10 41.68%

+ 85 98 .. i,|, , I 113 127 141 155168 183196 210 224 240 253 268 m/z-> Abundance O—T1 +— 20 40 60 80 100 120 140 160 180 200 #16522: Undecane, 3-methyl- 220 240 260 Mwa/MV/A 57

43 27.40 27.60 27.80 28.00 5000 m/z 85.10 34.72% . 71 CD

O-T 29

I— -I-r "I ' 1 ' ["1 1 991 1 1’112*14126 141 155 170 ■ 1 i ' ■ ■ 1 i ■ ■ ■ ■ i ■ ■ ■ ■ i • ■ ■ ■ i ' ■ ■ ■ I ' ■ asMus/ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #112333: Octadecane 57 27.40 27.60 27.80 28.00 43 m/z 41.10 32.21% 71 5000 85 VWwyw/”yWw/W"W 29 0 ■ 1 4 |.. I ,. Ji. 4 . X 113127 141 155 169,183 197,211 225 239 254 ., m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 27.40 27.60 27.80 28.00

9570.D 050102.M Mon May 13 11:46:45 2002 Page 10

NYC-WTC_000023037

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NYC-WTC_000023037Source: NYC Law Department, mirrored locally

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