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GCMS analysis results for sample AE11158, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11158 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024665–000024680

Folder label: “GCMS X 5/13/02 A 5/15/02

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Scanned page image, NYC-WTC_000024679
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020515\11158.D Vial: 10 Acq On : 15 May 2002 8:43 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 9 Octadecane, 3-methyl- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

44.63 0.35 ug/1 20098 Perylene-d12 43.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane, 3-methyl- 268 C19H40 006561-44-0 43 2 Squalane 422 C30H62 000111-01-3 43 3 Decane, 3-methyl- 156 C11H24 013151-34-3 43 4 Dod) cane, 2,6,10-trimethyl- 212 C15H32 003891-98-3 38 Abundance/ Scan 7072 (44.631 min): 11158.D (-7066) (-) m/ z 57.10 100.00% 57

5000

857 4 4 4

1 177 208 239 265 429 adAAuaAnhaalsnaantbhakaiy 44.20 44.40 44.60 44.80 45.00 — | | m/z 71.05 53.11% mz-> 50 100 150 200 250 300 350 400 Abundance #16301: Octadecane, 3-methyl- 57

5000 85 AhAaanAunk 44.20 44.40 44.60 44.80 45.00 239 m/Z 43.00 51.84% I J ' I TT113 141169) 211 1 268 m/z-> 50 100 150 200 250 300 350 400 Abundance #112383: Squalane 57 AbmudAAanMAtldinisann 44.20 44.40 44.60 44.80 45.00 5000 m/z 55.10 41.46% 85 113 144 183 239 ,

mz-> 28. , 1 1J J1 ■ 1141, 1 ' ‘ I 50 ■ 1 । 1 ,1211 1 1 1 j ' 11 1267 100 ’ 1 1 1 150 200 250 308 337 300 350 37g 407 400 Abundance #112364: Decane, 3-methyl- 57 44.20 44.40 44.60 44.80 45.00 m/z 69.10 28.49% 5000 29 85

/z- > ' 1 " *i '*i 1 50 100 127 [ 156 150 200 250 300 350 400 MU 44.20 44.40 44.60 44.80 45.00

11158.D SCANO20507.M Thu May 16 09:53:08 2002 Page 11

NYC-WTC_000024679

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NYC-WTC_000024679Source: NYC Law Department, mirrored locally

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