GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7115.D vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise : Multiplr: i.'oo MS Integration Params: LSCINT.P

Quant Method C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title Quantitation For Method 508gcscan Library C:\DATABASE\WILEY7N. L

Peak Number 19 Tridecane, 2-methyl- $$ 2-M... Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T.

37.72 5.58 ug/L 515015 Perylene-dl2 34.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tridecane, 2-methyl- $$ 2-Methyl... 198 C14H30 001560-96-9 64 2 Tetradecane, 6,9-dimethyl- 226 C16H34 055045-13-1 64 3 1-Iodoundecane $$ Undecane, 1-iodo- 282 C11H23I 004282-44-4 64 4 Pentadecane (CAS) $$ n-Pentadeca... 212 C15H32 _____ 000629-62-9 59 Abundance Scan 5896 (37.722 min): 7115.D (-) m/z 57.10 100.00% 5(7

85 5000

4 113 _^A4OJA6O3A8O_38J0O__ m/z 85.10 54.36% 0 'n/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #113308; Tridecane, 2-methyl- $$ 2-Methyltridecane $5 2-Me... 57

553 41 85 37.40 37.60 37.80 38.00 m/z 71.10 47.81% 155 113

Tl/Z-> 0 2 0 A /I... 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #154934: Tetradecane, 6,9-dimethyl- 57

37.40 37.60 37.80 38.00 5000 41 m/z 43.10 43.22%

85 155

'n/z-> OHn 0 XmX IT 139 i 180197 226 'I'"' I 20 40 60 80 100 120 140 160 180 200 220 240 260 280 TT I'III IH ■II..II I

Abundance #227492; 1-lodoundecane $S Undecane, 1-iodo- 5(7 37.40 37.60 37.80 38.00 m/z 55.10 23.42%

5000 4' 85

m/2-> 0 0 dll I ■'13129 T 183 211 1 • ’" I" " f'"' I'' ” I" ■ ■) ” " 20 40 60 80 100 120 140 160 180 200 220 240 260 280 282 37.40 37.60 37.80 38.00

7115.D 5080402BB.M Mon Apr 15 18:16:43 2002 Page 22

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